4-CHLORO-2-PHENYLQUINAZOLINE(6484-25-9) 1H NMR
Product Name4-CHLORO-2-PHENYLQUINAZOLINE
CAS6484-25-9
Molecular FormulaC14H9ClN2
Molecular Weight240.69
InChIInChI=1S/C14H9ClN2/c15-13-11-8-4-5-9-12(11)16-14(17-13)10-6-2-1-3-7-10/h1-9H
InChIKey OBHKONRNYCDRKM-UHFFFAOYSA-N
SmilesN1=C2C(C=CC=C2)=C(Cl)N=C1C1=CC=CC=C1
-
MassMS-NW-7040 4-chloro-2-phenylquinazoline C14H9ClN2 (Mass of molecular ion: 240)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 4.1 27.0 1.2 39.5 1.7 50.0 4.8 51.0 9.4 52.0 1.8 63.0 1.4 74.0 1.7 75.0 8.8 76.0 8.3 77.0 19.1 78.0 1.5 89.0 1.0 100.0 1.0 102.0 19.8 102.5 1.6 103.0 5.0 104.0 3.0 119.0 2.3 120.0 5.6 120.5 1.1 121.0 1.9 151.0 1.7 177.0 2.0 205.0 100.0 206.0 16.0 207.0 1.3 222.0 1.8 240.0 39.6 241.0 6.6 242.0 13.4 243.0 2.1
400 MHz in CDCl3
-
1H NMR 399.65 MHz C14 H9 Cl N2 0.042 g : 0.5 ml CDCl3 4-chloro-2-phenylquinazoline 
Assign. Shift(ppm)
A 8.575 B 8.194 C 8.049 D 7.879 E 7.604 F 7.51
Hz ppm Int.3436.28 8.599 39 3431.70 8.587 387 3430.79 8.585 300 3429.57 8.582 276 3427.43 8.577 431 3424.22 8.569 474 3421.94 8.563 437 3418.43 8.554 75 3279.42 8.206 283 3278.66 8.204 289 3274.99 8.195 36 3271.18 8.186 308 3270.42 8.184 310 3221.59 8.062 304 3213.20 8.041 382 3157.20 7.900 185 3155.82 7.897 190 3150.33 7.883 233 3148.80 7.879 339 3147.43 7.876 185 3141.78 7.862 176 3140.41 7.858 170 3046.88 7.624 203 3045.81 7.622 214 3039.86 7.607 216 3038.64 7.604 343 3037.57 7.601 231 3031.62 7.586 177 3030.55 7.584 178 3014.37 7.543 42 3013.31 7.540 40 3012.70 7.539 38 3008.42 7.528 170 3006.90 7.524 188 3004.91 7.519 574 3003.69 7.516 574 3000.34 7.508 882 2997.89 7.502 1000 2994.23 7.493 140 2990.88 7.484 40
in CDCl3
KBr disc
nujol mull
