4β-Pentyl-1α-cyclohexanecarboxylic acid p-tolyl ester(67589-69-9) ¹³C NMR

Mass

MS-NW-4493          
p-tolyl trans-4-pentylcyclohexanecarboxylate
C19H28O2            (Mass of molecular ion:    288)

   Source Temperature: 230 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       2.5
      27.0       7.1
      28.0       2.3
      29.0      10.7
      39.0       7.1
      40.0       1.3
      41.0      27.3
      42.0       2.2
      43.0      17.3
      51.0       2.5
      52.0       1.6
      53.0       6.9
      54.0       8.1
      55.0      43.8
      56.0       3.0
      57.0      16.3
      65.0       3.4
      66.0       1.4
      67.0      21.6
      68.0       5.0
      69.0      38.5
      70.0       2.6
      71.0      21.0
      72.0       1.2
      77.0       9.3
      78.0       2.7
      79.0       9.5
      80.0       3.3
      81.0      29.4
      82.0       8.1
      83.0      87.9
      84.0       6.1
      85.0       5.2
      90.0       1.5
      91.0       5.9
      92.0       1.1
      93.0       1.9
      95.0      11.8
      96.0       9.6
      97.0     100.0
      98.0       8.0
     107.0      18.2
     108.0      89.0
     109.0      15.6
     110.0       2.5
     111.0      25.5
     112.0       2.5
     123.0       1.4
     124.0       1.2
     137.0       1.0
     138.0       1.3
     149.0       3.5
     151.0       1.5
     152.0       1.4
     153.0      45.0
     154.0       5.6
     162.0       1.8
     180.0      51.5
     181.0      30.3
     182.0       3.9
     288.0       7.3
     289.0       1.7

Assign. Shift(ppm) A 7.149 B 6.930 C 2.449 D 2.327 E 2.119 F 1.864 G 1.542 J 1.37 to 1.18 K 1.20 L 0.96 M 0.889

     Hz     ppm     Int.

   2864.87   7.169     36
   2864.14   7.167     41
   2862.18   7.162    237
   2861.45   7.160    268
   2860.11   7.157    117
   2859.38   7.155     94
   2855.71   7.146     95
   2853.52   7.141    317
   2852.78   7.139    294
   2850.83   7.134     56
   2850.22   7.132     49
   2776.25   6.947     60
   2773.68   6.941    442
   2771.73   6.936    138
   2767.09   6.924    121
   2765.26   6.920    366
   2762.57   6.913     50
    991.58   2.482     60
    987.92   2.472     35
    982.79   2.460     61
    979.25   2.451    120
    975.71   2.442     64
    970.58   2.429     38
    967.04   2.420     65
    963.50   2.411     34
    930.05   2.328   1000
    855.10   2.140     90
    853.76   2.137     87
    851.68   2.132     92
    846.56   2.119     50
    841.43   2.106     99
    839.48   2.101     91
    838.01   2.097     93
    752.44   1.883     91
    751.46   1.881     90
    749.76   1.877     97
    743.90   1.862     44
    743.65   1.861     44
    738.89   1.849     98
    735.96   1.842     93
    636.84   1.594     47
    633.42   1.585     44
    623.66   1.561    118
    620.12   1.552    105
    611.21   1.530    107
    607.67   1.521    102
    597.90   1.497     40
    594.48   1.488     36
    532.35   1.333     78
    531.62   1.331     74
    526.12   1.317    150
    524.90   1.314    142
    522.58   1.308    142
    519.53   1.300    203
    517.09   1.294    190
    511.72   1.281    208
    508.18   1.272    210
    506.59   1.268    190
    505.98   1.267    191
    504.03   1.262    156
    502.56   1.258    170
    499.39   1.250    118
    495.97   1.242    133
    492.07   1.232     95
    487.55   1.220    149
    483.40   1.210    119
    480.83   1.204    123
    476.07   1.192     61
    473.75   1.186     87
    468.14   1.172     31
    405.88   1.016     49
    402.47   1.008     49
    392.70   0.983    108
    389.28   0.975     94
    381.47   0.955     83
    378.30   0.947     90
    368.16   0.922     52
    364.50   0.913     75
    362.43   0.907    252
    355.59   0.890    718
    351.44   0.880     52
    348.27   0.872    285