5,N-DIMETHYL-3-(4-FLUOROPHENYL)-4-ISOXAZOLECARBOXAMIDE)(67764-99-2) IR1

Mass

MS-IW-0832          
3-(p-fluorophenyl)-N,5-dimethyl-4-isoxazolecarboxamide
C12H11FN2O2         (Mass of molecular ion:    234)

   Source Temperature: 130 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       1.3
      28.0       1.2
      30.0       1.6
      43.0      38.4
      44.0       1.2
      57.0       1.5
      58.0       4.3
      75.0       4.1
      82.0       4.5
      84.0       1.0
      94.0       1.8
      95.0       8.4
      96.0       2.0
      97.0       1.4
     107.0       4.8
     108.0       1.8
     109.0      11.2
     110.0       1.2
     111.0       4.7
     112.0       1.1
     117.0       1.1
     121.0       3.6
     122.0       2.9
     123.0       3.5
     124.0       8.7
     125.0      13.4
     126.0       1.0
     133.0       1.4
     134.0      11.8
     135.0       6.6
     136.0       1.6
     146.0       1.2
     147.0       2.7
     148.0       8.1
     149.0       1.6
     160.0       1.5
     161.0       5.8
     162.0      88.9
     163.0      14.0
     164.0       4.2
     175.0       1.3
     176.0       1.1
     177.0       5.4
     191.0       4.8
     192.0       5.1
     204.0       4.6
     205.0       2.0
     206.0       1.0
     216.0       1.2
     217.0       1.1
     219.0      10.4
     220.0       1.4
     233.0       6.9
     234.0     100.0
     235.0      14.8
     236.0       1.5

Assign. Shift(ppm) A 7.601 B 7.185 C 5.60 D 2.811 E 2.658

     Hz     ppm     Int.

   3045.04   7.620    127
   3042.97   7.615     67
   3039.79   7.607    143
   3038.33   7.603     91
   3037.72   7.601     91
   3036.25   7.598    155
   3033.20   7.590     74
   3031.01   7.585    142
   2879.88   7.207    139
   2877.81   7.201     57
   2873.05   7.189     73
   2871.34   7.185    235
   2869.38   7.180     73
   2864.75   7.169     55
   2862.55   7.163    126
   2239.14   5.603     30
   1126.22   2.819    521
   1121.34   2.806    526
   1062.26   2.658   1000