3-METHOXY-4-NITROBENZYL ALCOHOL(80866-88-2) 13C NMR
Product Name3-METHOXY-4-NITROBENZYL ALCOHOL
CAS80866-88-2
Molecular FormulaC8H9NO4
Molecular Weight183.16
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MassMS-NW-8075 3-methoxy-4-nitrobenzyl alcohol C8H9NO4 (Mass of molecular ion: 183)
Source Temperature: 170 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 5.0 17.0 1.6 18.0 7.7 26.0 1.3 27.0 8.1 28.0 7.4 29.0 9.1 30.0 7.4 31.0 11.2 37.0 2.3 38.0 6.3 39.0 28.3 40.0 6.9 41.0 9.3 42.0 1.4 43.0 3.1 45.0 2.0 47.0 1.1 50.0 12.6 51.0 26.7 52.0 12.2 53.0 24.9 54.0 5.3 55.0 8.8 59.0 4.9 61.0 2.6 62.0 8.4 63.0 20.8 64.0 7.1 65.0 39.0 66.0 35.4 67.0 9.7 68.0 2.7 69.0 2.1 74.0 5.8 75.0 6.2 76.0 9.5 77.0 68.1 78.0 26.0 79.0 43.3 80.0 59.7 81.0 14.3 82.0 8.4 83.0 1.0 89.0 39.4 90.0 7.1 91.0 9.3 92.0 7.6 93.0 14.3 94.0 25.6 95.0 5.6 96.0 5.6 97.0 9.9 98.0 1.2 104.0 2.2 105.0 40.1 106.0 15.6 107.0 12.8 108.0 39.5 109.0 12.9 110.0 3.5 119.0 6.0 120.0 2.8 121.0 8.9 122.0 6.2 123.0 2.4 124.0 19.0 125.0 2.3 134.0 1.1 135.0 5.4 136.0 28.1 137.0 5.8 138.0 1.7 150.0 1.0 151.0 1.1 152.0 3.1 153.0 16.0 154.0 4.0 166.0 3.4 167.0 2.3 182.0 1.7 183.0 100.0 184.0 12.4 185.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O4 0.040 g : 0.5 ml CDCl3 3-methoxy-4-nitrobenzyl alcohol 
Assign. Shift(ppm)
A 7.820 B 7.135 C 6.960 D 4.76 E 3.955 F 2.53
Hz ppm Int.704.44 7.866 132 696.25 7.775 160 639.19 7.138 125 638.75 7.133 127 628.50 7.018 57 627.81 7.010 91 627.00 7.001 79 626.19 6.992 77 619.50 6.918 74 618.63 6.908 66 617.88 6.900 64 617.19 6.892 40 426.81 4.766 165 354.25 3.956 1000
in CDCl3
KBr disc
nujol mull
