N-[3-(diethylamino)propyl]-4-ethoxybenzamide monohydrochloride(81028-99-1) IR2
Molecular FormulaC16H27ClN2O2
Molecular Weight314.85078
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MassMS-NW-9592 N-(3-(diethylamino)propyl)-p-ethoxybenzamide hydrochloride C16H26N2O2 HCl (Mass of molecular ion: 278)
Source Temperature: 210 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 1.8 28.0 1.7 29.0 1.7 30.0 4.3 36.0 6.8 38.0 2.2 42.0 1.5 44.0 1.4 56.0 2.6 57.0 1.1 58.0 7.1 65.0 2.1 70.0 1.2 71.0 1.9 72.0 24.6 73.0 1.4 84.0 14.2 85.0 1.6 86.0 100.0 87.0 6.6 93.0 3.1 98.0 2.3 100.0 6.7 112.0 1.7 113.0 1.2 119.0 1.4 120.0 1.2 121.0 10.4 149.0 19.3 150.0 2.2 165.0 1.9 166.0 1.7 178.0 1.9 206.0 15.7 207.0 3.1 208.0 1.5 249.0 27.9 250.0 6.0 263.0 2.0 278.0 7.1 279.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H26 N2 O2 0.036 g : 0.5 ml CDCl3 N-(3-(diethylamino)propyl)-p-ethoxybenzamide hydrochloride 
Assign. Shift(ppm)
A 11.15 B 8.51 C 8.002 D 6.875 E 4.034 F 3.578 G 3.21 to 3.04 J 2.171 K 1.407 L 1.353
Hz ppm Int.4454.50 11.147 42 3405.91 8.523 50 3400.27 8.509 94 3394.47 8.494 48 3205.26 8.021 52 3202.36 8.013 370 3200.38 8.008 124 3195.50 7.996 121 3193.36 7.991 394 3190.61 7.984 49 2754.82 6.894 52 2751.92 6.886 395 2749.94 6.881 127 2745.06 6.869 116 2743.07 6.864 389 2740.17 6.857 47 1622.77 4.061 113 1615.75 4.043 371 1608.89 4.026 372 1601.87 4.009 114 1438.60 3.600 65 1432.65 3.585 140 1426.54 3.570 140 1420.75 3.555 62 1278.84 3.200 31 1276.40 3.194 54 1272.13 3.184 67 1269.23 3.176 78 1262.97 3.161 166 1255.80 3.143 221 1251.22 3.131 195 1244.81 3.115 146 1239.93 3.103 117 1237.79 3.098 111 1232.60 3.085 111 1226.50 3.069 62 1225.43 3.067 59 1224.52 3.064 60 1219.33 3.051 42 880.89 2.205 38 873.87 2.187 91 867.61 2.171 112 861.36 2.156 81 569.46 1.425 413 562.44 1.408 830 555.57 1.391 407 547.94 1.372 501 540.77 1.354 1000 533.45 1.335 466
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
