1-METHYL-4-PIPERIDONE OXIME HYDROCHLORIDE(84540-61-4) ¹³C NMR

Mass

MS-IW-9139          
1-methyl-4-piperidone oxime hydrochloride
C6H12N2O HCl        (Mass of molecular ion:    128)

   Source Temperature: 170 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      15.0      12.1
      17.0       4.4
      18.0      23.6
      26.0      10.0
      27.0      20.0
      28.0      29.2
      29.0       6.7
      30.0       8.3
      31.0       1.4
      35.0       9.5
      36.0      84.7
      37.0       4.0
      38.0      29.5
      39.0       9.9
      40.0      11.8
      41.0      33.2
      42.0     100.0
      43.0      60.2
      44.0      59.6
      45.0       2.7
      46.0       6.2
      50.0       1.5
      51.0       4.0
      52.0       9.1
      53.0      10.3
      54.0      18.4
      55.0      12.2
      56.0      21.0
      57.0      24.0
      58.0       4.2
      65.0       1.0
      66.0       2.1
      67.0      13.1
      68.0      13.6
      69.0       8.0
      70.0      48.2
      71.0      13.8
      72.0       1.3
      73.0       2.0
      79.0       1.9
      80.0       3.1
      81.0       5.0
      82.0      11.6
      83.0       8.7
      84.0       5.4
      85.0      17.1
      86.0       4.2
      92.0       1.0
      93.0       1.0
      94.0       2.9
      95.0       3.6
      96.0      12.0
      97.0       2.7
      98.0      14.6
      99.0       1.3
     107.0       1.5
     108.0       2.3
     109.0      14.2
     110.0      15.8
     111.0      23.6
     112.0       4.7
     113.0       2.4
     127.0      30.4
     128.0      76.0
     129.0       5.9

Assign. Shift(ppm) A 10.7 B 3.3 B 2.6 C 2.749

     Hz     ppm     Int.

   4296.72  10.752     93
   1315.32   3.292     62
   1110.36   2.779     25
   1108.71   2.775     22
   1108.16   2.773     22
   1099.00   2.750   1000
   1026.83   2.570     34