Mass

MS-NW-7851          
2a,3,4,5-tetrahydrobenz(cd)indol-2(1H)-one
C11H11NO            (Mass of molecular ion:    173)

   Source Temperature: 190 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      27.0       3.0
      28.0       2.1
      38.0       1.4
      39.0       8.8
      40.0       1.2
      41.0       2.0
      50.0       3.1
      51.0       8.8
      52.0       4.0
      53.0       2.1
      57.5       1.9
      58.5       4.2
      62.0       2.1
      63.0       7.6
      64.0       4.7
      64.5       1.0
      65.0       7.2
      66.0       1.2
      70.5       2.5
      71.5       9.5
      72.0       2.2
      72.5       2.0
      74.0       1.3
      75.0       2.6
      76.0       3.0
      77.0       9.3
      78.0       3.3
      85.5       1.3
      86.5       3.2
      87.0       1.4
      88.0       1.3
      89.0       8.2
      90.0       5.7
      91.0       6.4
     101.0       1.6
     102.0       3.7
     103.0       5.8
     104.0       2.2
     113.0       1.1
     114.0       1.9
     115.0      17.7
     116.0       7.5
     117.0      13.7
     118.0       2.9
     126.0       1.3
     127.0      11.8
     128.0      14.1
     129.0       6.7
     130.0      52.1
     131.0       5.8
     132.0       1.9
     140.0       1.5
     141.0       1.0
     142.0       2.5
     143.0      11.9
     144.0      87.8
     145.0      77.1
     146.0       8.6
     154.0       1.6
     156.0       1.0
     171.0       1.1
     172.0       3.5
     173.0     100.0
     174.0      12.9
     175.0       1.0

Assign. Shift(ppm) A 8.93 B 7.103 C *1 6.779 D *1 6.688 E 3.325 F 2.886 G 2.623 J 2.419 K 2.12 L 1.89 M 1.365 J(M,E)=J(M,L)=12.1HZ J(M,J)=-12.1HZ J(M,K)=3.8HZ J(E,J)=5.4HZ J(F,G)=-17.6HZ J(J,K)=J(J,L)=3.9HZ

     Hz     ppm     Int.

   3569.09   8.931    365
   2852.17   7.137     31
   2846.92   7.124    409
   2846.07   7.122    477
   2839.11   7.104    869
   2838.38   7.103   1000
   2831.42   7.085    506
   2830.57   7.083    579
   2712.89   6.789    932
   2704.96   6.769    827
   2676.64   6.698    962
   2669.07   6.679    879
   1337.77   3.348    310
   1332.40   3.334    332
   1325.81   3.318    333
   1320.68   3.305    325
   1167.60   2.922    222
   1160.03   2.903    241
   1155.27   2.891     46
   1150.02   2.878    311
   1142.58   2.859    319
   1064.58   2.664    178
   1056.15   2.643    278
   1047.24   2.621    330
   1038.57   2.599    209
   1029.91   2.578    149
    979.49   2.451    162
    975.71   2.442    341
    974.24   2.438    242
    971.92   2.432    242
    970.34   2.428    364
    966.80   2.420    305
    963.50   2.411    370
    962.04   2.408    262
    959.59   2.402    242
    958.13   2.398    366
    954.22   2.388    181
    866.70   2.169     91
    864.50   2.164    115
    863.04   2.160    187
    860.84   2.154    204
    859.38   2.151    204
    857.06   2.145    195
    855.71   2.142    219
    852.91   2.135    239
    849.00   2.125    295
    846.80   2.119    280
    845.34   2.116    271
    843.02   2.110    253
    841.67   2.107    278
    839.36   2.101    245
    838.01   2.097    184
    835.69   2.092    162
    833.74   2.087    118
    825.68   2.067     30
    778.69   1.949     97
    774.66   1.939    106
    771.00   1.930    111
    768.55   1.924    128
    766.24   1.918    183
    764.65   1.914    213
    762.08   1.907    158
    760.86   1.904    193
    758.42   1.898    170
    756.84   1.894    224
    754.52   1.888    233
    752.20   1.883    242
    750.73   1.879    153
    748.29   1.873    192
    744.38   1.863    198
    742.19   1.858    148
    740.60   1.854    115
    738.04   1.847     96
    734.38   1.838     83
    730.47   1.828     73
    565.19   1.415    179
    561.40   1.405    190
    552.86   1.384    451
    549.19   1.375    443
    540.77   1.354    423
    536.99   1.344    407
    528.56   1.323    159
    524.78   1.314    143