10061-68-4

N,N'-二乙基-1,3-丙二胺(10061-68-4)核磁图(¹³CNMR)

产品名称:N,N'-二乙基-1,3-丙二胺

CAS:10061-68-4

分子式:C7H18N2

分子量: 130.23

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9731          
N,N'-diethyltrimethylenediamine
C7H18N2             (Mass of molecular ion:    130)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.0
      18.0       3.2
      27.0       4.7
      28.0      13.2
      29.0       8.8
      30.0      58.0
      31.0       1.0
      39.0       1.4
      41.0       6.7
      42.0       8.6
      43.0       4.6
      44.0      25.8
      45.0      12.9
      46.0       1.3
      50.0       6.3
      54.0       1.1
      56.0      18.5
      57.0       7.0
      58.0     100.0
      59.0       4.9
      68.0       1.2
      70.0      91.2
      71.0       6.7
      72.0      19.3
      73.0       1.5
      84.0       8.7
      85.0      72.6
      86.0       6.3
      87.0       6.7
     130.0       1.2
     131.0       2.2
     141.0       3.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₈ N₂	0.05 ml : 0.5 ml CDCl₃
N,N'-diethyltrimethylenediamine

    Assign.     Shift(ppm)

      A             2.676
      B             2.645
      C             1.691
      D             1.46
      E             1.105

     Hz     ppm     Int.

   1076.90   2.695    355
   1069.82   2.677    594
   1067.87   2.673    289
   1062.87   2.660    404
   1060.67   2.654    642
   1057.01   2.645     40
   1053.47   2.636    639
   1050.17   2.628     36
   1046.39   2.619    262
    689.82   1.727     56
    682.74   1.709    188
    675.66   1.691    244
    668.58   1.673    171
    661.74   1.656     53
    583.01   1.459    145
    448.97   1.124    610
    441.77   1.106   1000
    434.69   1.088    669

in CDCl3