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101-83-7

二环己胺(101-83-7)核磁图(13CNMR)

产品名称:二环己胺

CAS:101-83-7

分子式:C12H23N

分子量: 181.32

InChI:InChI=1S/C12H23N/c1-3-7-11(8-4-1)13-12-9-5-2-6-10-12/h11-13H,1-10H2

InChIKey: XBPCUCUWBYBCDP-UHFFFAOYSA-N

Smiles:C1(NC2CCCCC2)CCCCC1

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    Mass

    MS-NW-5522          
    dicyclohexylamine
    C12H23N             (Mass of molecular ion:    181)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       2.8
          28.0       4.1
          29.0       3.9
          30.0       4.4
          39.0       3.5
          41.0      12.6
          42.0       1.8
          43.0       3.5
          44.0       9.1
          53.0       2.0
          54.0       2.7
          55.0      12.5
          56.0      39.2
          57.0       1.9
          67.0       2.6
          68.0       1.9
          69.0       1.4
          70.0       2.7
          79.0       1.1
          81.0       3.1
          82.0       7.7
          83.0       5.0
          96.0       1.9
          98.0       4.9
         100.0       5.5
         110.0       2.7
         124.0       1.5
         125.0       1.6
         138.0     100.0
         139.0      10.9
         152.0       3.2
         180.0       1.1
         181.0      13.9
         182.0       1.9
    

400 MHz in CDCl3

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    1H NMR 399.65 MHz
    C12 H23 N 0.05 ml : 0.5 ml CDCl3
    dicyclohexylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.546 B 1.856 C 1.712 D 1.606 E 1.246 F 1.146 G 1.021 J 0.7

         Hz     ppm     Int.
    

       1040.65   2.604     30
       1040.04   2.603     30
       1038.94   2.600     31
       1032.10   2.583    213
       1028.44   2.574    386
       1024.66   2.564    257
       1021.61   2.557    423
       1017.82   2.547    747
       1014.04   2.538    437
       1011.11   2.530    266
       1007.32   2.521    414
       1003.54   2.512    230
        749.15   1.875    758
        746.70   1.869    791
        741.70   1.856    521
        736.57   1.844    811
        735.23   1.840    796
        733.89   1.837    819
        717.16   1.795     46
        715.45   1.791     44
        715.09   1.790     43
        714.72   1.789     43
        694.58   1.738    592
        691.16   1.730    803
        687.62   1.721    646
        681.40   1.705    718
        677.98   1.697    928
        675.54   1.691    706
        662.11   1.657     72
        660.64   1.654     68
        659.18   1.650     64
        658.81   1.649     64
        651.12   1.630    353
        649.41   1.625    400
        648.07   1.622    467
        646.48   1.618    374
        644.65   1.614    347
        639.16   1.600    372
        635.74   1.591    471
        632.20   1.582    341
        628.78   1.574    133
        534.55   1.338     31
        533.81   1.336     31
        530.03   1.327     41
        522.09   1.307    217
        518.80   1.299    310
        515.38   1.290    191
        509.77   1.276    527
        506.47   1.268    816
        503.42   1.260    473
        496.83   1.244    649
        493.77   1.236   1000
        490.97   1.229    614
        484.25   1.212    382
        481.20   1.205    595
        479.00   1.199    387
        474.98   1.189    299
        472.53   1.183    490
        469.60   1.176    306
        463.75   1.161    362
        460.69   1.153    681
        457.28   1.145    372
        451.78   1.131    245
        448.49   1.123    499
        445.07   1.114    262
        439.70   1.101    131
        436.16   1.092    194
        432.62   1.083    138
        426.03   1.067    433
        422.97   1.059    423
        413.33   1.035    865
        411.13   1.029    819
        402.71   1.008    736
        400.15   1.002    790
        390.75   0.978    288
        387.57   0.970    306
        379.15   0.949     33
        377.93   0.946     32
        294.56   0.738     47
    

in CDCl3

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CCl4 solution

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liquid film

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4880 A,200 M,liquid

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