103-67-3

N-甲基苄胺(103-67-3)Raman光谱

产品名称:N-甲基苄胺

CAS:103-67-3

分子式:C8H11N

分子量: 121.18

InChI:InChI=1S/C8H11N/c1-9-7-8-5-3-2-4-6-8/h2-6,9H,7H2,1H3

InChIKey: RIWRFSMVIUAEBX-UHFFFAOYSA-N

Smiles:C1(CNC)=CC=CC=C1

Mass

MS-NW-1310          
N-methylbenzylamine
C8H11N              (Mass of molecular ion:    121)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       3.7
      18.0       2.2
      27.0       2.8
      28.0      14.4
      29.0       1.0
      30.0      28.2
      38.0       2.0
      39.0      11.6
      40.0       1.1
      41.0       3.5
      42.0      45.4
      43.0      12.6
      44.0     100.0
      45.0       2.7
      50.0       5.3
      51.0      11.4
      52.0       3.5
      53.0       1.2
      58.0       9.2
      58.5       2.2
      59.5       1.5
      60.5       1.8
      62.0       2.1
      63.0       6.3
      64.0       1.9
      65.0      16.4
      66.0       1.2
      74.0       1.2
      75.0       1.1
      76.0       1.4
      77.0      11.0
      78.0       7.6
      79.0       6.0
      89.0       5.1
      90.0       2.2
      91.0      63.3
      92.0      13.5
      93.0       1.1
     104.0       3.9
     105.0       1.1
     106.0       6.0
     107.0       3.6
     108.0       1.9
     117.0       1.0
     118.0       5.6
     119.0       2.2
     120.0      98.6
     121.0      61.7
     122.0       5.3
     134.0       2.6
     135.0       4.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N	0.04 ml : 0.5 ml CDCl₃
N-methylbenzylamine

    Assign.     Shift(ppm)

      A          7.50 to 7.10
      B             3.741
      C             2.434
      D             2.20

     Hz     ppm     Int.

    660.44   7.375     32
    659.25   7.361     39
    658.69   7.355     37
    656.69   7.333    110
    655.94   7.325    146
    653.88   7.302    891
    651.94   7.280    161
    651.31   7.273    188
    649.06   7.248     91
    335.00   3.741    449
    218.00   2.435   1000
    197.00   2.200    232

in CDCl3