1066-50-8

二氯化乙基磷酸(1066-50-8)核磁图(¹³CNMR)

产品名称:二氯化乙基磷酸

CAS:1066-50-8

分子式:C2H5Cl2OP

分子量: 146.94

InChI:InChI=1S/C2H5Cl2OP/c1-2-6(3,4)5/h2H2,1H3

InChIKey: OWGJXSYVHQEVHS-UHFFFAOYSA-N

Smiles:C(P(Cl)(Cl)=O)C

Mass

MS-NW-9541          
ethylphosphonic dichloride
C2H5Cl2OP           (Mass of molecular ion:    146)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       3.3
      27.0      17.3
      28.0      10.4
      29.0      38.6
      36.0       1.3
      47.0      12.0
      48.0       2.0
      66.0       1.2
      82.0       1.8
      83.0      17.3
      85.0       5.7
     101.0       1.7
     103.0       1.1
     109.0       2.2
     110.0       1.5
     111.0      20.2
     113.0       6.3
     117.0       3.6
     118.0     100.0
     119.0       3.0
     120.0      64.9
     122.0      10.3
     145.0       2.9
     146.0       2.3
     147.0       2.8
     148.0       1.5
     149.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂ H₅ Cl₂ O P	0.05 ml : 0.5 ml CDCl₃
ethylphosphonic dichloride

    Assign.     Shift(ppm)

      A             2.634
      B             1.423
     
     J(P-31,B)=30.0HZ
     J(P-31,A)=14.8HZ

     Hz     ppm     Int.

   1070.92   2.680    187
   1063.35   2.661    519
   1055.91   2.643    618
   1048.46   2.624    634
   1043.09   2.611     37
   1041.02   2.605    531
   1033.57   2.587    196
    596.68   1.494     37
    591.19   1.480    546
    583.74   1.461    986
    579.22   1.450     37
    576.17   1.442    529
    568.24   1.422     37
    567.14   1.420     46
    566.65   1.418     47
    561.04   1.404    552
    553.59   1.386   1000
    548.22   1.372     46
    546.02   1.367    533
    540.77   1.354     33

in CDCl3