109705-14-8

1-氟-2,4,6-三甲基吡啶四氟化硼(109705-14-8)质谱(MS)

产品名称:1-氟-2,4,6-三甲基吡啶四氟化硼

CAS:109705-14-8

分子式:C8H11BF5N

分子量: 226.98

InChI:InChI=1S/C8H11FN.BF4/c1-6-4-7(2)10(9)8(3)5-6;2-1(3,4)5/h4-5H,1-3H3;/q+1;-1

InChIKey: RRNLYYDDEUOXBB-UHFFFAOYSA-N

Smiles:[N+]1(F)C(C)=CC(C)=CC=1C.[B-](F)(F)(F)F

Mass

MS-IW-7206          
1-fluoro-2,4,6-trimethylpyridinium tetrafluoroborate
C8H11BF5N           (Mass of molecular ion:    227)

   Source Temperature: 180 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      18.0       1.4
      20.0       7.4
      27.0       4.7
      28.0       2.6
      33.0       1.2
      38.0       2.5
      39.0      12.8
      40.0       2.0
      41.0       3.7
      42.0       5.3
      48.0       7.8
      49.0      31.8
      50.0       3.2
      51.0       8.6
      52.0       4.7
      53.0       5.7
      54.0       1.1
      57.0       2.6
      59.0       1.3
      62.0       1.4
      63.0       4.1
      64.0       1.9
      65.0       4.5
      66.0       2.4
      67.0       1.2
      68.0       2.7
      70.0       1.1
      75.0       1.3
      76.0       1.1
      77.0      19.5
      78.0       7.2
      79.0      32.3
      80.0       5.7
      81.0       1.5
      83.0       1.4
      91.0       7.3
      92.0       4.3
      93.0       4.0
      94.0       1.7
      95.0       2.1
      96.0       1.7
      97.0      13.0
      98.0       3.2
     103.0       1.0
     104.0      16.6
     105.0       2.1
     106.0      19.2
     107.0       3.2
     109.0       1.7
     111.0       1.4
     117.0       1.1
     118.0       8.2
     119.0       2.7
     120.0      19.6
     121.0      71.4
     122.0       8.0
     124.0       5.9
     137.0       1.0
     138.0      10.7
     139.0     100.0
     140.0      10.2
     157.0       3.8

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈ H₁₁ B F₅ N	0.041 g : 0.5 ml DMSO-d₆
1-fluoro-2,4,6-trimethylpyridinium tetrafluoroborate

    Assign.     Shift(ppm)

      A             7.582
      B             2.635
      C             2.500

     Hz     ppm     Int.

   3030.27   7.583    228
   3029.79   7.582    226
   1053.22   2.636   1000
    998.78   2.500    493

in DMSO-d6

KBr disc

nujol mull

更多供应商

Capot Chemical Co., Ltd