(E)4-氯-3-甲氧基-2-丁稀酸甲酯(110104-60-4)核磁图(¹³CNMR)

Mass

MS-IW-5081          
methyl (E)-4-chloro-3-methoxy-2-butenoate
C6H9ClO3            (Mass of molecular ion:    164)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       8.4
      26.0       1.8
      27.0       9.2
      28.0       2.3
      29.0       4.2
      31.0       3.0
      37.0       1.2
      38.0       3.2
      39.0      15.3
      40.0       8.6
      41.0       6.1
      42.0       3.8
      43.0       3.1
      45.0       3.7
      47.0       2.0
      49.0       4.8
      51.0       2.2
      53.0       3.9
      55.0      19.0
      56.0       1.8
      57.0       1.7
      59.0      24.7
      61.0       1.7
      67.0      14.5
      68.0      25.8
      69.0      15.9
      70.0       1.1
      71.0       1.2
      73.0       4.2
      75.0       3.5
      77.0       3.5
      79.0       1.6
      83.0      26.6
      84.0       1.5
      85.0       2.9
      89.0       2.2
      91.0       1.0
      96.0      11.5
      97.0       5.7
      98.0       3.5
      99.0       7.0
     101.0       3.7
     102.0       5.1
     103.0       4.3
     104.0       1.8
     105.0       5.6
     106.0       1.3
     107.0       1.4
     114.0       1.2
     115.0       3.8
     123.0       2.9
     129.0       1.8
     132.0      89.0
     133.0     100.0
     134.0      34.0
     135.0      38.2
     136.0       2.3
     137.0       2.2
     147.0       3.3
     164.0      32.5
     165.0       4.3
     166.0      10.7
     167.0       1.4

Parameter ppm Hz D(A) 5.160 D(B) 4.657 D(C) *1 3.724 D(D) *1 3.717

     Hz     ppm     Int.

   1547.99   5.160    323
   1397.10   4.657    646
   1117.19   3.724   1000
   1115.11   3.717   1000