1119-34-2

L-精氨酸盐酸盐(1119-34-2)核磁图(¹³CNMR)

产品名称:L-精氨酸盐酸盐

CAS:1119-34-2

分子式:C6H15ClN4O2

分子量: 210.66

InChI:InChI=1/C6H14N4O2.ClH/c7-4(5(11)12)2-1-3-10-6(8)9;/h4H,1-3,7H2,(H,11,12)(H4,8,9,10);1H/t4-;/s3

InChIKey: KWTQSFXGGICVPE-NDILARRWNA-N

Smiles:C([C@H](N)C(=O)O)CCNC(=N)N.Cl |&1:1,r|

Mass

MS-NW-0316          
L-arginine monohydrochloride
C6H14N4O2 HCl       (Mass of molecular ion:    174)

   Source Temperature: 180 °C
   Sample Temperature: 280 °C
   Direct, 75 eV

      15.0       1.3
      16.0      28.6
      17.0      39.1
      18.0      45.1
      26.0       1.5
      27.0       5.7
      28.0      13.8
      29.0       2.3
      30.0      14.3
      31.0       1.5
      35.0      12.9
      36.0     100.0
      37.0       4.2
      38.0      32.7
      39.0       7.0
      40.0       2.5
      41.0      12.1
      42.0      16.4
      43.0      37.4
      44.0      31.3
      50.0       1.5
      51.0       2.3
      52.0       2.9
      53.0       3.2
      54.0       5.9
      55.0       6.5
      56.0      15.8
      57.0       4.7
      58.0       7.2
      59.0      17.2
      60.0       1.0
      63.0       1.0
      64.0       1.3
      65.0       4.5
      66.0       2.3
      67.0       3.5
      68.0       8.1
      69.0      22.6
      70.0      12.2
      71.0       1.3
      72.0       1.1
      75.0       1.3
      76.0       1.0
      77.0       1.4
      78.0       2.1
      79.0       1.9
      80.0       3.1
      81.0       2.9
      82.0       5.7
      83.0       5.0
      84.0       2.8
      85.0       3.1
      86.0       2.0
      87.0       1.3
      91.0       1.3
      92.0       3.3
      93.0       2.7
      94.0       2.5
      95.0       3.0
      96.0       2.3
      97.0       3.0
      98.0       3.2
      99.0       1.7
     104.0       1.0
     105.0       1.1
     106.0       1.3
     107.0       2.3
     108.0       2.0
     109.0       3.8
     110.0       6.2
     111.0       4.2
     112.0       3.7
     113.0       1.7
     114.0       1.2
     118.0       1.4
     119.0       2.9
     120.0       5.4
     121.0       2.8
     122.0       1.9
     123.0       2.9
     124.0       1.3
     125.0       1.4
     126.0       2.0
     132.0       1.1
     133.0       2.4
     134.0       3.1
     135.0       3.4
     136.0       4.6
     137.0       9.1
     138.0       8.7
     139.0       3.5
     145.0       1.4
     146.0       1.9
     147.0       1.9
     148.0       1.7
     149.0       2.1
     150.0       2.5
     151.0       3.7
     152.0       3.0
     153.0       1.1
     161.0       1.3
     162.0       1.5
     163.0       1.8
     164.0       3.4
     165.0       3.9
     166.0       3.1
     167.0       2.8
     172.0       1.3
     173.0       2.4
     174.0       1.3
     175.0       1.5
     176.0       2.2
     177.0       1.8
     178.0       2.2
     179.0       1.1
     187.0       1.1
     189.0       2.1
     190.0       3.1
     191.0       1.8
     192.0       1.1
     202.0       1.1
     204.0       1.0
     205.0       1.1
     206.0       1.7
     244.0       1.1

90 MHz in D2O

¹H NMR	89.56 MHz
C₆ H₁₄ N₄ O₂	0.049 g : 0.5 ml D₂O
L-arginine monohydrochloride

    Assign.     Shift(ppm)

      B             3.786
      C             3.261
      D          2.08 to 1.510
     
     THE SOLVENT SIGNAL REMOVED.

     Hz     ppm     Int.

    345.13   3.854    261
    343.19   3.832    102
    339.44   3.791    579
    336.13   3.754     74
    333.69   3.726    353
    333.56   3.725    353
    303.06   3.384     40
    301.75   3.370     55
    298.69   3.336    515
    291.94   3.260   1000
    285.69   3.190    474
    282.50   3.155     53
    169.56   1.894    514
    166.56   1.860    533
    165.94   1.853    523
    164.50   1.837    583
    163.50   1.826    549
    158.38   1.769    543
    152.56   1.704    395

in D2O