盐酸-N-(3-苯氨基-2-丙烯亚基)苯胺(123071-42-1)核磁图(¹³CNMR)

Mass

MS-KW-0192          
N-(3-anilinoallylidene)aniline monohydrochloride
C15H14N2 HCl        (Mass of molecular ion:    222)

   Source Temperature: 180 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      18.0       1.1
      28.0       2.3
      35.0       1.4
      36.0      19.6
      38.0       6.9
      39.0       3.2
      50.0       1.8
      51.0      11.8
      52.0       2.1
      63.0       1.2
      65.0       3.9
      66.0       2.7
      76.0       2.0
      77.0      31.0
      78.0       4.0
      89.0       1.2
      90.0       1.9
      91.0       5.9
      92.0       2.4
      93.0       9.1
     102.0       2.7
     103.0       6.7
     104.0       7.8
     111.0       7.2
     111.5       1.2
     116.0       2.2
     117.0       5.4
     118.0       9.0
     119.0       3.2
     128.0       4.9
     129.0       8.7
     130.0      22.1
     131.0       2.4
     143.0       2.5
     144.0       3.1
     145.0      10.2
     146.0       1.1
     180.0       1.8
     193.0       1.1
     194.0       2.7
     195.0       1.9
     204.0       1.1
     205.0       1.0
     206.0       5.0
     219.0       4.2
     220.0       1.9
     221.0      99.2
     222.0     100.0
     223.0      15.9
     224.0       1.3

Assign. Shift(ppm) A 12.8 B 9.056 C 7.48 D 7.25 E 6.589

     Hz     ppm     Int.

   5120.42  12.813     72
   3621.02   9.061     78
   3609.85   9.033     75
   2996.24   7.498    124
   2989.83   7.482   1000
   2987.81   7.477    516
   2983.42   7.466    365
   2978.29   7.453     50
   2976.64   7.449     62
   2974.62   7.444     87
   2906.12   7.272     66
   2904.10   7.267    106
   2901.17   7.260     86
   2899.89   7.257    105
   2897.69   7.251    122
   2895.50   7.246     95
   2891.65   7.236     66
   2889.27   7.230     44
   2645.11   6.619     53
   2633.57   6.590    102
   2622.03   6.561     50