13019-22-2

9-十烯-1-醇(13019-22-2)核磁图(¹HNMR)

产品名称:9-十烯-1-醇

CAS:13019-22-2

分子式:C10H20O

分子量: 156.27

Mass

MS-NW-7567          
9-decen-1-ol
C10H20O             (Mass of molecular ion:    156)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0      13.2
      28.0       3.2
      29.0      18.4
      31.0      18.1
      39.0      18.0
      40.0       3.4
      41.0      65.1
      42.0      12.7
      43.0      22.5
      44.0       4.3
      45.0       3.7
      51.0       1.3
      53.0       7.8
      54.0      51.9
      55.0     100.0
      56.0      14.9
      57.0      11.6
      58.0       1.6
      65.0       1.4
      66.0       4.2
      67.0      57.1
      68.0      55.8
      69.0      24.8
      70.0       5.6
      71.0       5.5
      72.0       1.4
      73.0       1.1
      79.0       2.3
      80.0       1.4
      81.0      42.5
      82.0      32.4
      83.0       9.2
      84.0       2.1
      85.0       3.3
      86.0       1.0
      95.0      20.6
      96.0      15.7
      97.0       5.2
      99.0       2.3
     109.0       8.7
     110.0       7.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₂₀ O	0.05 ml : 0.5 ml CDCl₃
9-decen-1-ol

    Assign.     Shift(ppm)

      A             5.80
      B             4.95
      C             4.91
      D             3.62
      E             2.29
      F             2.04
      G             1.46
      J             1.31

     Hz     ppm     Int.

    534.81   5.972     47
    531.44   5.934     30
    524.94   5.862     69
    517.63   5.780     76
    514.25   5.742     45
    511.06   5.707     43
    507.75   5.670     87
    501.25   5.597     47
    457.13   5.105     44
    455.69   5.089     87
    454.69   5.077     94
    453.38   5.063    135
    451.94   5.047     71
    447.75   5.000     81
    446.69   4.988    131
    445.44   4.974    101
    444.31   4.962     76
    443.19   4.949     44
    439.94   4.913     38
    436.69   4.876    165
    436.19   4.871    155
    434.81   4.855     95
    433.44   4.840     32
    323.50   3.613    149
    204.25   2.281     46
    179.88   2.009    123
    117.69   1.315   1000

in CDCl3