13360-63-9

N-乙基正丁胺(13360-63-9)核磁图(¹³CNMR)

产品名称:N-乙基正丁胺

CAS:13360-63-9

分子式:C6H15N

分子量: 101.19

InChI:InChI=1S/C6H15N/c1-3-5-6-7-4-2/h7H,3-6H2,1-2H3

InChIKey: QHCCDDQKNUYGNC-UHFFFAOYSA-N

Smiles:C(NCC)CCC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3270          
n-ethylbutylamine
C6H15N              (Mass of molecular ion:    101)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.0
      18.0       1.2
      27.0       5.0
      28.0       5.1
      29.0       7.7
      30.0      32.9
      39.0       1.8
      41.0       4.0
      42.0       2.7
      43.0       1.5
      44.0       9.6
      56.0       2.6
      57.0       2.6
      58.0     100.0
      59.0       3.7
      86.0       2.4
     100.0       2.1
     101.0       9.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₅ N	0.04 ml : 0.5 ml CDCl₃
N-ethylbutylamine

    Assign.     Shift(ppm)

      A             2.63
      B             2.62
      C          1.69 to 1.14
      D             1.105
      E             0.99
      F             0.92

     Hz     ppm     Int.

    248.25   2.772     52
    246.31   2.751     38
    241.13   2.693    178
    234.06   2.614    253
    227.19   2.537    130
    140.38   1.568     46
    138.13   1.543     62
    135.50   1.513     71
    132.38   1.479    145
    129.25   1.444    179
    128.06   1.430    190
    126.13   1.409    158
    124.94   1.396    193
    123.06   1.375    130
    121.81   1.361    141
    119.19   1.331     84
    117.06   1.308     65
    115.69   1.292     70
    112.63   1.258     50
    109.88   1.227     56
    106.06   1.185    454
    102.81   1.148     41
    102.69   1.147     41
     98.94   1.105   1000
     91.88   1.026    490
     89.69   1.002    206
     88.75   0.991    243
     84.88   0.948    100
     82.38   0.920    454
     79.94   0.893    121
     76.31   0.853     77
     74.94   0.837     87
     73.00   0.816     46

in CDCl3