13513-82-1

甲氧基二甲基苄甲醇(13513-82-1)核磁图(¹³CNMR)

产品名称:甲氧基二甲基苄甲醇

CAS:13513-82-1

分子式:C9H12O2

分子量: 152.19

Mass

MS-NW-7298          
(+-)-2-methoxy-alpha-methylbenzyl alcohol
C9H12O2             (Mass of molecular ion:    152)

   Source Temperature: 200 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.6
      28.0       1.1
      29.0       1.0
      38.0       1.4
      39.0       5.8
      41.0       1.0
      43.0      10.8
      45.0       1.9
      50.0       3.1
      51.0       7.6
      52.0       1.6
      53.0       1.6
      55.0       1.0
      62.0       1.3
      63.0       4.3
      64.0       2.4
      65.0       8.2
      66.0       2.0
      68.5       2.8
      74.0       1.3
      75.0       1.5
      76.0       3.5
      77.0      22.2
      78.0       4.9
      79.0       6.9
      89.0       1.7
      90.0       1.0
      91.0      10.0
      92.0       3.3
      93.0       2.9
      94.0      10.4
      95.0       1.2
     103.0       2.9
     104.0       2.0
     105.0       7.4
     107.0      52.2
     108.0       6.1
     109.0      28.3
     110.0       2.6
     119.0       4.1
     120.0       1.5
     121.0      12.2
     122.0       5.9
     133.0       1.4
     134.0       1.8
     135.0       5.9
     136.0       1.0
     137.0     100.0
     138.0       9.2
     151.0       1.6
     152.0      26.7
     153.0       3.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₂ O₂	0.05 ml : 0.5 ml CDCl₃
(+-)-2-methoxy-alpha-methylbenzyl alcohol

    Assign.     Shift(ppm)

      A             7.32
      B             7.22
      C             6.91
      D             6.83
      E             5.070
      F             3.791
      G             2.9
      J             1.457

     Hz     ppm     Int.

    661.06   7.382     52
    659.19   7.361     64
    653.94   7.302     80
    652.00   7.281    105
    647.13   7.226     93
    645.13   7.204     64
    639.44   7.140     87
    637.44   7.118     60
    627.44   7.006     65
    626.19   6.992     82
    620.00   6.923     74
    618.88   6.911     97
    615.56   6.874    115
    612.88   6.844     45
    611.50   6.828     36
    607.69   6.786     67
    606.56   6.773     59
    457.44   5.108     65
    450.94   5.036     67
    339.56   3.792   1000
    133.44   1.490    519
    126.94   1.418    494

in CDCl3