137-43-9

溴代环戊烷(137-43-9)红外图谱(IR1)

产品名称:溴代环戊烷

CAS:137-43-9

分子式:C5H9Br

分子量: 149.03

InChI:InChI=1S/C5H9Br/c6-5-3-1-2-4-5/h5H,1-4H2

InChIKey: BRTFVKHPEHKBQF-UHFFFAOYSA-N

Smiles:C1(Br)CCCC1

Mass

MS-NW-1112          
bromocyclopentane
C5H9Br              (Mass of molecular ion:    148)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       5.0
      28.0       1.8
      38.0       1.3
      39.0      11.0
      40.0       2.5
      41.0      43.7
      42.0       3.7
      53.0       2.9
      67.0       7.6
      68.0       4.2
      69.0     100.0
      70.0       5.6

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₅ H₉ Br	0.05 ml : 0.5 ml CDCl₃
bromocyclopentane

    Assign.     Shift(ppm)

      A             4.448
      B          2.12 to 2.05
      C     *1      1.89
      D     *1      1.65

     Hz     ppm     Int.

   1786.99   4.472    146
   1782.96   4.462    304
   1781.86   4.459    343
   1777.59   4.448    552
   1773.56   4.438    308
   1772.46   4.436    337
   1768.31   4.425    151
    855.10   2.140     48
    852.91   2.135     56
    851.93   2.132     37
    849.85   2.127     82
    847.29   2.121    133
    844.73   2.114     95
    841.31   2.106    268
    838.87   2.100    327
    835.69   2.092    461
    833.37   2.086    874
    830.44   2.078    685
    829.10   2.075    753
    827.76   2.072   1000
    825.20   2.065    836
    822.39   2.058    772
    819.82   2.052    623
    815.31   2.041    188
    814.58   2.039    181
    813.11   2.035    150
    810.55   2.029    127
    808.96   2.025    123
    807.74   2.022    102
    805.30   2.016     62
    803.71   2.012     51
    780.03   1.952     95
    775.51   1.941    102
    771.61   1.931    100
    770.75   1.929     94
    769.29   1.925    194
    766.97   1.920    249
    764.28   1.913    275
    761.47   1.906    546
    758.67   1.899    341
    756.47   1.893    428
    755.37   1.891    332
    753.78   1.887    449
    749.02   1.875    328
    745.73   1.866    168
    744.63   1.864    146
    740.97   1.855     80
    738.53   1.848     57
    736.45   1.843     78
    727.05   1.820     34
    680.79   1.704     91
    679.69   1.701     87
    676.39   1.693     97
    674.56   1.688    136
    674.19   1.687    135
    671.02   1.680    200
    669.19   1.675    291
    668.09   1.672    358
    666.50   1.668    298
    664.31   1.663    364
    663.21   1.660    432
    660.77   1.654    502
    659.55   1.651    447
    658.33   1.648    404
    656.86   1.644    377
    655.64   1.641    316
    653.44   1.636    330
    651.49   1.631    184
    650.51   1.628    201
    645.87   1.617    103
    645.26   1.615    111
    639.77   1.601     76
    638.18   1.597     33

¹H NMR	89.56 MHz
C₅ H₉ Br	0.04 ml : 0.5 ml CDCl₃
bromocyclopentane

    Assign.     Shift(ppm)

      A             4.45
      B             2.07
      C             1.76

     Hz     ppm     Int.

    403.56   4.507    204
    399.06   4.456    302
    394.56   4.406    252
    183.13   2.045    954
    178.63   1.995   1000
    162.94   1.820    323
    153.25   1.712    375

in CDCl3