142817-71-8

2,4,6-TRIS(1-CHLOROETHYL)-1,3,5-TRIOXANE(142817-71-8)核磁图(¹³CNMR)

产品名称:2,4,6-TRIS(1-CHLOROETHYL)-1,3,5-TRIOXANE

CAS:142817-71-8

分子式:C9H15Cl3O3

分子量: 277.57

Mass

MS-KW-0512          
2,4,6-tris(1-chloroethyl)-1,3,5-trioxane
C9H15Cl3O3          (Mass of molecular ion:    276)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      26.0       2.2
      27.0      12.2
      28.0      10.7
      29.0      25.9
      39.0       1.3
      41.0       1.2
      55.0       1.1
      56.0       4.3
      57.0      20.0
      58.0       2.1
      63.0       8.1
      64.0       4.4
      65.0       3.0
      66.0       1.4
      91.0       5.3
      92.0       6.0
      93.0     100.0
      94.0       5.4
      95.0      31.6
      96.0       1.0
     183.0       1.5
     185.0      10.5
     187.0       6.3
     189.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉H₁₅Cl₃O₃	0.038 g : 0.5 ml CDCl₃
2,4,6-tris(1-chloroethyl)-1,3,5-trioxane

    Assign.     Shift(ppm)

     A           4.984
     B           4.025
     C           1.537

     Hz     ppm     Int.

   1995.00   4.991    414
   1993.54   4.987     84
   1992.68   4.985     77
   1990.61   4.980    402
   1989.14   4.976     72
   1988.29   4.974     59
   1911.02   4.781      4
   1906.87   4.770      4
   1621.34   4.056     49
   1616.95   4.045     62
   1614.51   4.039    146
   1612.31   4.033     40
   1610.23   4.028    157
   1607.79   4.022    151
   1605.47   4.016     39
   1603.40   4.011    148
   1600.96   4.005     52
   1599.61   4.002     29
   1596.68   3.994     47
   1592.78   3.985      8
    839.73   2.101      5
    681.40   1.705      8
    674.57   1.688      8
    632.21   1.582     49
    617.19   1.544   1000
    610.36   1.527    956
    551.52   1.380      8
    544.68   1.363      8

in CDCl3