14352-61-5

乙酸甲酯环己酯(14352-61-5)核磁图(¹HNMR)

产品名称:乙酸甲酯环己酯

CAS:14352-61-5

分子式:C9H16O2

分子量: 156.22

Mass

MS-NW-7609          
methyl cyclohexylacetate
C9H16O2             (Mass of molecular ion:    156)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       3.6
      27.0       4.3
      29.0       3.6
      31.0       1.7
      39.0       5.9
      40.0       1.1
      41.0      11.2
      42.0       1.1
      43.0      24.9
      44.0       1.1
      53.0       3.1
      54.0       3.8
      55.0      16.7
      56.0       1.1
      59.0       2.7
      67.0       5.6
      68.0       1.5
      74.0     100.0
      75.0      29.9
      76.0       1.4
      79.0       1.5
      80.0       2.7
      81.0       5.5
      82.0       3.8
      83.0       3.5
      95.0       1.3
      97.0       4.1
     113.0       2.0
     124.0       1.1
     125.0       5.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₆ O₂	0.05 ml : 0.5 ml CDCl₃
methyl cyclohexylacetate

    Assign.     Shift(ppm)

      A             3.657
      B             2.185
      C          1.77 to 1.68
      D             1.27
      E             1.15
      F             0.965

     Hz     ppm     Int.

   1461.79   3.658   1000
    876.95   2.195    311
    870.00   2.177    305
    518.19   1.297     41
    515.99   1.292     45
    514.89   1.289     56
    511.72   1.281     40
    505.25   1.265     58
    502.20   1.257     68
    499.15   1.249     46
    492.68   1.233     31
    489.75   1.226     39
    474.12   1.187     30
    465.70   1.166     30
    462.16   1.157     42
    450.20   1.127     44
    403.32   1.010     32
    400.51   1.003     31
    391.48   0.980     67
    389.28   0.975     65
    388.31   0.972     65
    379.88   0.951     52
    377.32   0.945     61
    374.63   0.938     31

in CDCl3