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1530-87-6

1-氰基哌啶(1530-87-6)Raman光谱

产品名称:1-氰基哌啶

CAS:1530-87-6

分子式:C6H10N2

分子量: 110.16

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    Mass

    MS-NW-8577          
    1-piperidinecarbonitrile
    C6H10N2             (Mass of molecular ion:    110)
    

       Source Temperature: 250 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          15.0       2.5
          26.0       3.0
          27.0      15.6
          28.0      24.9
          29.0      10.9
          30.0       1.9
          38.0       1.2
          39.0      16.2
          40.0       4.0
          41.0      45.2
          42.0     100.0
          43.0      27.7
          44.0       2.8
          51.0       1.5
          52.0       1.2
          53.0      10.6
          54.0      13.2
          55.0      48.6
          56.0      13.8
          57.0      22.3
          65.0       1.5
          67.0      11.2
          68.0       6.8
          69.0      56.1
          70.0       4.4
          81.0       3.8
          82.0       9.6
          83.0       3.5
          92.0       2.2
          95.0       4.6
         109.0      53.7
         110.0      73.8
         111.0       9.3
    

90 MHz in CDCl3

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    1H NMR 89.56 MHz
    C6 H10 N2 0.05 ml : 0.5 ml CDCl3
    1-piperidinecarbonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.19 B 1.68 C 1.61

         Hz     ppm     Int.
    

        295.81   3.303     38
        295.31   3.298     45
        287.81   3.214    431
        285.50   3.188    612
        280.00   3.127    461
        273.69   3.056     45
        272.69   3.045     37
        162.44   1.814     39
        161.31   1.802     44
        158.88   1.775     77
        157.81   1.763     78
        156.25   1.745     99
        152.88   1.708    262
        149.69   1.672    426
        146.56   1.637    800
        145.31   1.623   1000
        143.75   1.606    940
        141.94   1.585    818
        134.63   1.504     64
        134.31   1.500     59
        132.63   1.481     40
        132.06   1.475     38
        131.38   1.467     37
    

in CDCl3

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liquid film

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