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1576-35-8

对甲苯磺酰肼(1576-35-8)红外图谱(IR2)

产品名称:对甲苯磺酰肼

CAS:1576-35-8

分子式:C7H10N2O2S

分子量: 186.23

InChI:InChI=1S/C7H10N2O2S/c1-6-2-4-7(5-3-6)12(10,11)9-8/h2-5,9H,8H2,1H3

InChIKey: ICGLPKIVTVWCFT-UHFFFAOYSA-N

Smiles:C1(S(NN)(=O)=O)=CC=C(C)C=C1

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    Mass

    MS-NW-4854          
    p-toluenesulfonohydrazide
    C7H10N2O2S          (Mass of molecular ion:    186)
    

       Source Temperature: 190 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          17.0       1.5
          18.0       8.3
          27.0       1.9
          28.0       4.1
          29.0       6.0
          30.0       5.5
          31.0      56.3
          38.0       1.5
          39.0      14.5
          40.0       1.2
          41.0       4.7
          45.0       2.5
          48.0       1.1
          50.0       3.1
          51.0       5.9
          52.0       2.0
          53.0       1.5
          62.0       2.1
          63.0       7.9
          64.0       2.3
          65.0      36.7
          66.0       2.4
          67.0       1.4
          77.0      10.3
          78.0       2.9
          79.0       7.4
          80.0       3.3
          89.0       6.7
          90.0       4.1
          91.0     100.0
          92.0      84.4
          93.0      16.9
          94.0       1.1
         106.0       2.9
         107.0       9.1
         108.0       7.6
         111.0       1.5
         123.0       2.5
         124.0       3.2
         139.0      20.4
         140.0       3.5
         141.0       1.1
         155.0       4.2
         156.0      25.1
         157.0      48.6
         158.0       5.7
         159.0       2.6
         186.0      16.5
         187.0       1.6
    

400 MHz in DMSO-d6

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    1H NMR 399.65 MHz
    C7 H10 N2 O2 S 0.039 g : 0.5 ml DMSO-d6
    p-toluenesulfonohydrazide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.32 B 7.702 C 7.405 D 4.0 E 2.389

         Hz     ppm     Int.
    

       3325.68   8.322     96
       3082.64   7.714    322
       3074.46   7.693    361
       2963.38   7.415    315
       2955.20   7.395    276
       1608.89   4.026     22
        955.08   2.390   1000
    

in CDCl3

in DMSO-d6

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KBr disc

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nujol mull

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