16239-18-2

1,6-二溴-2-萘酚(16239-18-2)质谱(MS)

产品名称:1,6-二溴-2-萘酚

CAS:16239-18-2

分子式:C10H6Br2O

分子量: 301.96

InChI:InChI=1S/C10H6Br2O/c11-7-2-3-8-6(5-7)1-4-9(13)10(8)12/h1-5,13H

InChIKey: VKESFYLPKHQOOA-UHFFFAOYSA-N

Smiles:C1(Br)=C2C(C=C(Br)C=C2)=CC=C1O

Mass

MS-NW-9349          
1,6-dibromo-2-naphthol
C10H6Br2O           (Mass of molecular ion:    300)

   Source Temperature: 160 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      18.0       2.0
      55.0       1.0
      56.0       5.0
      56.5       4.7
      57.0       3.1
      62.0       1.6
      63.0       3.6
      70.5       1.8
      71.0       4.3
      86.0       1.4
      87.0       1.9
      88.0       1.5
      96.0       2.6
      96.5       3.6
      97.0       2.9
      97.5       3.4
     110.0       1.4
     111.0       1.4
     113.0      13.6
     114.0       6.3
     141.0       4.0
     142.0       2.0
     150.0       4.8
     151.0       9.4
     151.5       1.0
     152.0       4.7
     192.0      10.0
     193.0       5.9
     194.0      10.3
     195.0       5.5
     222.0       1.4
     224.0       1.0
     273.0       1.4
     300.0      51.1
     301.0       6.0
     302.0     100.0
     303.0      11.1
     304.0      49.5
     305.0       5.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₆ Br₂ O	0.049 g : 0.5 ml CDCl₃
1,6-dibromo-2-naphthol

    Assign.     Shift(ppm)

      A             7.885
      B             7.841
      C             7.590
      D             7.580
      E             7.238
      F             5.92

     Hz     ppm     Int.

   3152.34   7.888    730
   3150.39   7.883    754
   3138.67   7.854    571
   3129.64   7.831    670
   3038.09   7.602    539
   3034.55   7.594    561
   3032.59   7.589    550
   3029.30   7.580    618
   3025.51   7.571    474
   3023.56   7.566    465
   2896.97   7.249   1000
   2888.18   7.227    849
   2364.87   5.918    823

in CDCl3