壬二腈(1675-69-0)核磁图(¹³CNMR)

Mass

MS-IW-7343          
azelanitrile
C9H14N2             (Mass of molecular ion:    150)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.3
      18.0       1.3
      26.0       1.8
      27.0      15.6
      28.0      10.0
      29.0      13.8
      30.0       4.6
      38.0       1.3
      39.0      19.4
      40.0       4.5
      41.0      79.8
      42.0      15.0
      43.0       8.5
      44.0       2.1
      51.0       2.2
      52.0       3.4
      53.0       8.2
      54.0      41.3
      55.0      65.5
      56.0       5.5
      57.0       1.3
      65.0       1.7
      66.0       2.5
      67.0      12.9
      68.0      15.7
      69.0      59.4
      70.0       3.7
      77.0       2.2
      79.0       3.0
      80.0       3.1
      81.0       7.5
      82.0     100.0
      83.0      90.6
      84.0       5.5
      91.0       1.8
      93.0      10.4
      94.0       4.9
      95.0       2.4
      96.0      24.2
      97.0       5.4
     107.0       1.3
     108.0       1.7
     110.0      51.8
     111.0       4.2
     121.0       3.3
     122.0       2.6
     149.0       1.5
     151.0       2.7

Assign. Shift(ppm) A 2.361 B 1.668 C 1.477 D 1.383

     Hz     ppm     Int.

    950.68   2.379    550
    948.12   2.373     45
    943.60   2.362   1000
    936.52   2.344    569
    681.88   1.707     76
    675.05   1.690    205
    667.11   1.670    264
    659.79   1.651    257
    652.59   1.633    115
    605.83   1.516     84
    598.51   1.498    170
    596.31   1.493    131
    591.43   1.480    225
    590.45   1.478    205
    585.57   1.466    125
    583.01   1.459    197
    575.93   1.442    106
    566.89   1.419     31
    563.60   1.411     94
    559.94   1.402     80
    556.88   1.394    111
    556.03   1.392     94
    549.56   1.376    100
    546.14   1.367     44
    545.17   1.365     45
    543.58   1.361     46
    541.02   1.354     54