Phenothiazine, 10-[3-(dimethylamino)-2-methylpropyl]-2-methoxy-, maleate (1:1) (8CI)(17086-29-2)红外图谱(IR2)

Mass

MS-IW-3599          
10-(3-dimethylamino-2-methylpropyl)-2-methoxyphenothiazine maleate
C19H24N2OS C4H4O4   (Mass of molecular ion:    328)

   Source Temperature: 180 °C
   Sample Temperature: 200 °C
   Direct, 75 eV

      18.0       4.0
      26.0       4.8
      27.0       2.3
      28.0       1.5
      29.0       1.3
      30.0       2.2
      39.0       1.1
      41.0       1.8
      42.0       4.0
      43.0       1.8
      44.0       3.4
      45.0       3.9
      53.0       1.2
      54.0       4.5
      55.0       2.4
      57.0       1.5
      58.0     100.0
      59.0       5.8
      63.0       1.0
      69.0       1.3
      70.0       1.2
      71.0       1.4
      72.0       5.2
      77.0       1.0
      84.0       4.3
      85.0       1.6
      86.0       2.0
      98.0       1.7
      99.0       2.3
     100.0      16.9
     101.0       1.3
     141.0       1.0
     167.0       2.2
     184.0       1.1
     185.0       7.8
     186.0       3.0
     198.0       1.9
     199.0       1.6
     210.0       4.7
     211.0       1.1
     214.0       1.2
     227.0       1.5
     228.0       9.3
     229.0      10.8
     230.0       2.0
     242.0       8.6
     243.0       5.4
     244.0       1.2
     268.0       3.5
     269.0       3.1
     270.0       2.8
     282.0       5.6
     283.0       7.5
     284.0       1.7
     328.0      46.0
     329.0      10.3
     330.0       3.3

Assign. Shift(ppm) A 9. B 7.24 C 7.22 D 7.110 E 7.11 F 6.996 G 6.686 J 6.617 K 6.074 L *1 3.933 M *1 3.79 N 3.761 P *2 3.130 Q *2 3.036 R 2.721 S 2.35 T 1.051 J(L,M)=13.9HZ J(L,S)=6.8HZ J(M,S)=8.0HZ J(P,Q)=12.8HZ J(P,S)=4.5HZ J(Q,S)=8.4HZ

     Hz     ppm     Int.

   2901.91   7.262     30
   2896.05   7.247     38
   2894.58   7.243     54
   2893.85   7.241     55
   2889.27   7.230     79
   2887.99   7.227     93
   2886.52   7.223     60
   2881.58   7.211     94
   2880.29   7.208     65
   2846.22   7.122    164
   2844.03   7.117     73
   2837.80   7.101    183
   2803.73   7.016     42
   2802.63   7.013     43
   2796.22   6.997     69
   2795.49   6.995     66
   2788.89   6.979     35
   2787.79   6.976     34
   2673.86   6.691     87
   2671.30   6.685    105
   2649.87   6.631     73
   2647.49   6.625     61
   2641.44   6.610     66
   2638.88   6.603     60
   2427.51   6.075   1000
   1569.92   3.929     32
   1563.14   3.912     32
   1527.79   3.823     30
   1519.92   3.804     33
   1503.43   3.762    739
   1248.46   3.124     36
   1243.88   3.113     35
   1222.64   3.060     31
   1214.21   3.039     34
   1087.46   2.722    295
    423.30   1.060    200
    416.89   1.044    199