2-氯-3-甲氧基丙脒盐酸盐(175136-99-9)红外图谱(IR1)

Mass

MS-IW-2760          
2-chloro-3-methoxypropionamidine hydrochloride
C4H9ClN2O HCl       (Mass of molecular ion:    136)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       4.0
      17.0       1.1
      18.0       4.8
      26.0       1.1
      27.0       4.2
      28.0       6.7
      29.0       4.5
      30.0       9.9
      31.0       3.1
      33.0       2.6
      35.0       3.8
      36.0      32.3
      37.0       1.3
      38.0      11.0
      40.0       1.0
      41.0       2.4
      42.0       7.8
      43.0      55.7
      44.0       2.8
      45.0      29.6
      49.0       1.2
      52.0       2.3
      54.0       4.5
      58.0       2.5
      59.0       1.2
      60.0       5.5
      61.0       1.0
      62.0      16.6
      63.0       1.0
      64.0       6.4
      68.0       1.4
      69.0      17.4
      70.0       1.5
      71.0      14.3
      75.0       2.1
      76.0       1.3
      78.0       1.1
      84.0      27.9
      85.0       4.6
      86.0       1.3
      88.0       1.2
     101.0     100.0
     102.0       5.3
     104.0       2.9
     105.0       1.4
     106.0       1.1

Assign. Shift(ppm) A *1 9.70 B *1 9.44 C 5.176 D *2 3.946 E *2 3.818 F 3.348 J(D,E)=-11.0HZ J(C,D)=7.5HZ J(C,E)=6.1HZ

     Hz     ppm     Int.

   3877.87   9.704     72
   3772.43   9.440     69
   2075.50   5.194     42
   2069.24   5.178     65
   2068.18   5.175     59
   2062.07   5.160     45
   1587.37   3.972     48
   1579.90   3.954     49
   1576.39   3.945     69
   1569.06   3.927     66
   1533.81   3.838     66
   1527.71   3.823     70
   1522.98   3.811     54
   1516.88   3.796     47
   1338.04   3.349   1000