乙基二氯硅烷(1789-58-8)核磁图(¹³CNMR)

Mass

MS-KW-0100          
dichloroethylsilane
C2H6Cl2Si           (Mass of molecular ion:    128)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.9
      27.0       7.5
      28.0       5.6
      29.0      11.6
      36.0       2.8
      53.0       2.9
      63.0      30.9
      64.0       7.0
      65.0      16.7
      66.0       2.7
      67.0       2.3
      91.0       1.9
      92.0      17.9
      93.0       7.5
      94.0       6.4
      95.0       2.7
      98.0      60.9
      99.0     100.0
     100.0      46.3
     101.0      67.3
     102.0      10.9
     103.0      12.4
     113.0       1.2
     115.0       1.3
     125.0       1.0
     126.0       1.5
     127.0      67.9
     128.0      21.2
     129.0      47.5
     130.0      13.8
     131.0      10.1
     132.0       2.5
     133.0       1.5
     135.0       1.0
     143.0       1.0
     145.0       1.4
     173.0       1.5
     175.0       1.0

Assign. Shift(ppm) A 5.497 B 1.19 C 1.13

     Hz     ppm     Int.

   2198.36   5.501    265
   2196.90   5.498    490
   2195.31   5.494    293
    490.36   1.227     45
    488.89   1.224     44
    486.94   1.219     61
    485.23   1.215    102
    483.89   1.211     63
    483.15   1.209     45
    480.96   1.204    195
    479.37   1.200    301
    477.54   1.195    197
    473.63   1.186    157
    472.66   1.183    342
    472.05   1.182    378
    471.07   1.179    333
    470.46   1.178    298
    467.65   1.171    210
    466.19   1.167    336
    464.60   1.163    260
    462.40   1.158     68
    458.25   1.147    546
    457.15   1.144    558
    451.54   1.130   1000
    448.97   1.124    179
    445.19   1.114    255
    443.36   1.110    202
    442.63   1.108    140
    439.70   1.101    100