2,2,2-三氯乙酯二氯磷酸(18868-46-7)核磁图(¹³CNMR)

Mass

MS-NW-9779          
2,2,2-trichloroethyl dichlorophosphate
C2H2Cl5O2P          (Mass of molecular ion:    264)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       3.1
      29.0       2.3
      36.0       4.1
      38.0       1.3
      47.0      10.4
      48.0       1.6
      49.0       9.0
      51.0       2.8
      60.0       4.2
      61.0      11.6
      62.0       1.8
      63.0       5.4
      77.0      20.0
      79.0       6.4
      82.0       2.9
      83.0       3.7
      84.0       1.6
      85.0       2.0
      95.0       9.9
      96.0       9.1
      97.0       8.2
      98.0       8.3
      99.0       5.1
     100.0       1.2
     101.0       2.6
     103.0       1.0
     113.0       1.0
     117.0      37.6
     119.0      28.3
     121.0       6.8
     130.0       1.5
     131.0       3.4
     132.0       1.4
     133.0       3.1
     135.0      21.4
     137.0      13.1
     139.0       2.1
     147.0     100.0
     148.0       1.2
     149.0      64.3
     151.0      10.5
     229.0      24.2
     231.0      31.0
     233.0      15.1
     235.0       3.3

Assign. Shift(ppm) A 4.807 J(A,P-31)=9.1HZ

     Hz     ppm     Int.

   1926.03   4.820    982
   1916.87   4.797   1000