1932-04-3

1,2-二哌啶基乙烷(1932-04-3)质谱(MS)

产品名称:1,2-二哌啶基乙烷

CAS:1932-04-3

分子式:C12H24N2

分子量: 196.33

InChI:InChI=1S/C12H24N2/c1-3-7-13(8-4-1)11-12-14-9-5-2-6-10-14/h1-12H2

InChIKey: UYMQPNRUQXPLCY-UHFFFAOYSA-N

Smiles:C(N1CCCCC1)CN1CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8886          
1,2-dipiperidinoethane
C12H24N2            (Mass of molecular ion:    196)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       1.1
      30.0       1.1
      41.0       4.4
      42.0       3.5
      44.0       2.9
      55.0       4.5
      56.0       1.5
      69.0       2.3
      70.0       2.4
      96.0       1.4
      98.0     100.0
      99.0       7.0
     112.0       2.0
     196.0       1.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₂₄ N₂	0.04 ml : 0.5 ml CDCl₃
1,2-dipiperidinoethane

    Assign.     Shift(ppm)

      A             2.477
      B             2.41
      C          1.84 to 1.21

     Hz     ppm     Int.

    221.81   2.477   1000
    215.88   2.411    149
    210.31   2.349    145
    151.81   1.696     24
    146.06   1.631     61
    145.00   1.620     57
    141.50   1.580     86
    140.19   1.566     98
    133.63   1.493    152
    127.44   1.423     41
    125.50   1.402     31
    122.94   1.373     24

in CDCl3