对叔丁基氯苄(19692-45-6)核磁图(¹³CNMR)

Mass

MS-NW-7776          
p-tert-butylbenzyl chloride
C11H15Cl            (Mass of molecular ion:    182)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.4
      27.0       3.7
      29.0       3.1
      39.0       8.8
      41.0      12.1
      50.0       2.2
      51.0       5.6
      52.0       1.5
      53.0       2.6
      55.0       1.4
      57.0       1.5
      62.0       1.7
      63.0       5.3
      64.0       4.6
      64.5       1.0
      65.0       6.5
      66.0       1.6
      75.0       1.4
      76.0       1.0
      77.0       5.3
      78.0       2.2
      79.0       1.5
      89.0       3.9
      90.0       1.3
      91.0      25.1
      92.0       2.6
     102.0       1.3
     103.0       4.2
     104.0       4.0
     105.0       4.4
     115.0      10.6
     116.0       4.9
     117.0      12.7
     118.0       2.1
     119.0       1.5
     127.0       1.3
     128.0       2.4
     129.0       2.1
     131.0      22.4
     132.0      10.4
     133.0       2.8
     139.0      18.0
     140.0       1.9
     141.0       6.0
     147.0      11.0
     148.0       1.9
     149.0       3.8
     151.0       1.6
     167.0     100.0
     168.0      11.5
     169.0      32.1
     170.0       3.7
     182.0      23.5
     183.0       2.9
     184.0       7.8
     185.0       1.2

Assign. Shift(ppm) A 7.35 B 7.30 C 4.540 D 1.304

     Hz     ppm     Int.

    657.56   7.343    160
    656.81   7.334    121
    656.13   7.327    139
    406.75   4.542    176
    116.81   1.305   1000