2051-98-1

5-溴苊(2051-98-1)核磁图(¹HNMR)

产品名称:5-溴苊

CAS:2051-98-1

分子式:C12H9Br

分子量: 233.1

Mass

MS-KW-0501          
5-bromoacenaphthene
C12H9Br             (Mass of molecular ion:    232)

   Source Temperature: 120 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      39.0       1.3
      50.0       2.5
      51.0       2.8
      61.0       1.1
      62.0       3.5
      63.0      12.9
      63.5       1.8
      74.0       4.1
      75.0      10.9
      75.5      12.3
      76.0      41.5
      76.5      21.0
      77.0       4.4
      86.0       1.7
      87.0       2.0
      98.0       2.1
      99.0       1.9
     100.0       1.0
     101.0       1.3
     102.0       1.0
     116.0       2.8
     117.0       2.5
     125.0       1.6
     126.0       3.7
     127.0       1.9
     149.0       1.0
     150.0      10.8
     151.0      20.8
     152.0      65.7
     153.0     100.0
     154.0      13.1
     231.0       2.2
     232.0      66.8
     233.0      10.9
     234.0      65.1
     235.0       8.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₉ Br	0.034 g : 0.5 ml CDCl₃
5-bromoacenaphthene

    Assign.     Shift(ppm)

      A             7.742
      B             7.621
      C             7.514
      D             7.287
      E             7.087
      F             3.37
      G             3.29

     Hz     ppm     Int.

   3099.00   7.755    468
   3098.27   7.753    500
   3090.58   7.734    570
   3089.97   7.732    604
   3049.68   7.631    928
   3046.26   7.623     72
   3042.36   7.613   1000
   3010.50   7.533    522
   3007.32   7.525     77
   3003.54   7.516    609
   3002.20   7.513    491
   2995.24   7.495    510
   2915.28   7.295    485
   2908.45   7.278    431
   2837.40   7.100    302
   2836.06   7.097    612
   2834.59   7.093    356
   2829.96   7.082    292
   2828.61   7.078    581
   2827.27   7.075    336
   1354.74   3.390    307
   1353.52   3.387    326
   1349.00   3.376    542
   1346.19   3.369    363
   1344.85   3.366    390
   1343.38   3.362    441
   1341.92   3.358    617
   1340.94   3.356    628
   1320.31   3.304    750
   1319.09   3.301    511
   1317.63   3.297    437
   1316.28   3.294    412
   1314.70   3.290    356
   1313.23   3.286    556
   1312.26   3.284    534
   1308.96   3.276    282
   1307.62   3.272    411
   1306.27   3.269    280

in CDCl3