2155-94-4

二甲基烯丙基胺(2155-94-4)质谱(MS)

产品名称:二甲基烯丙基胺

CAS:2155-94-4

分子式:C5H11N

分子量: 85.15

InChI:InChI=1S/C5H11N/c1-4-5-6(2)3/h4H,1,5H2,2-3H3

InChIKey: GBCKRQRXNXQQPW-UHFFFAOYSA-N

Smiles:C(N(C)C)C=C

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3224          
N,N-dimethylallylamine
C5H11N              (Mass of molecular ion:     85)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       8.0
      18.0       1.1
      26.0       1.0
      27.0       3.1
      28.0       2.8
      29.0       2.4
      30.0       7.4
      38.0       1.8
      39.0      10.5
      40.0       2.0
      41.0      23.5
      42.0      41.9
      43.0       7.7
      44.0      11.6
      55.0       1.0
      56.0       1.3
      57.0       1.4
      58.0     100.0
      59.0       4.1
      68.0       3.2
      69.0       1.3
      70.0      11.3
      78.0       2.6
      82.0       2.5
      83.0       1.6
      84.0      24.6
      85.0      40.5
      86.0       2.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₁ N	0.04 ml : 0.5 ml CDCl₃
N,N-dimethylallylamine

    Assign.     Shift(ppm)

      A             5.833
      B             5.14
      C             5.10
      D             2.910
      E             2.219
     
     J(A,B)=17.3HZ. J(A,C)=9.7HZ. J(A,D)=6.4HZ. J(B,D)=J(C,D)=1.1HZ.

     Hz     ppm     Int.

    512.13   5.719     42
    470.00   5.248     33
    468.88   5.236     56
    467.56   5.221     30
    463.56   5.176     50
    462.44   5.164     37
    453.56   5.065     51
    451.94   5.047     64
    450.81   5.034     30
    263.63   2.944     78
    262.50   2.931     50
    257.25   2.873     73
    256.06   2.860     45
    198.81   2.220   1000

in CDCl3