2304-30-5

四丁基氯化膦(2304-30-5)红外图谱(IR1)

产品名称:四丁基氯化膦

CAS:2304-30-5

分子式:C16H36ClP

分子量: 294.88

InChI:InChI=1S/C16H36P.ClH/c1-5-9-13-17(14-10-6-2,15-11-7-3)16-12-8-4;/h5-16H2,1-4H3;1H/q+1;/p-1

InChIKey: IBWGNZVCJVLSHB-UHFFFAOYSA-M

Smiles:[P+](CCCC)(CCCC)(CCCC)CCCC.[Cl-]

Mass

MS-IW-9005          
tetrabutylphosphonium chloride
C16H36ClP           (Mass of molecular ion:    294)

   Source Temperature: 200 °C
   Sample Temperature: 230 °C
   Direct, 75 eV

      18.0       2.0
      25.0       1.1
      26.0       8.0
      27.0      22.0
      28.0      21.6
      29.0      34.9
      35.0       4.2
      36.0      35.6
      37.0       2.2
      38.0      12.9
      39.0      19.7
      40.0       3.4
      41.0      55.4
      42.0       5.6
      43.0       9.6
      44.0       1.3
      45.0       6.1
      46.0       1.5
      47.0       6.0
      48.0       7.3
      49.0       2.8
      50.0       3.0
      51.0       3.0
      52.0       1.6
      53.0       8.0
      54.0       7.9
      55.0      39.9
      56.0      13.7
      57.0      14.8
      58.0       3.7
      59.0      13.1
      60.0       4.9
      61.0      37.0
      62.0      65.3
      63.0       3.5
      67.0       2.3
      68.0       1.3
      69.0       9.3
      71.0       6.0
      72.0       1.4
      73.0      10.1
      74.0      10.0
      75.0      11.1
      76.0      96.2
      77.0       4.2
      78.0       1.3
      79.0       1.0
      81.0       1.4
      83.0       4.3
      85.0       3.7
      86.0       2.1
      87.0       8.6
      88.0      13.9
      89.0      29.9
      90.0      17.9
      91.0       3.1
      92.0       1.2
      96.0       1.3
      97.0       1.7
      99.0       1.3
     100.0       1.5
     101.0       4.5
     102.0      10.5
     103.0      22.9
     104.0      37.3
     105.0       4.0
     113.0       1.0
     114.0       1.1
     115.0       5.7
     116.0       6.8
     117.0      10.2
     118.0      40.7
     119.0       3.1
     129.0       3.7
     130.0       3.7
     131.0      18.8
     132.0       6.2
     143.0       3.3
     144.0       3.2
     145.0      30.8
     146.0      26.5
     147.0       4.0
     157.0       2.5
     158.0       1.6
     159.0       4.5
     160.0      17.5
     161.0       2.1
     171.0       4.2
     172.0       1.2
     173.0      33.6
     174.0       5.9
     185.0       1.4
     187.0       7.7
     188.0       1.1
     199.0       3.0
     200.0       1.7
     201.0      62.5
     202.0      30.5
     203.0       4.9
     213.0       1.1
     215.0       1.7
     227.0       3.7
     229.0     100.0
     230.0      15.9
     231.0       1.4
     243.0       2.4
     243.5       2.3
     257.0      22.2
     258.0      17.7
     259.0      91.4
     260.0      16.0
     261.0       1.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₆ H₃₆ Cl P	0.05 ml : 0.5 ml DMSO-d₆
tetrabutylphosphonium chloride

    Assign.     Shift(ppm)

      A             2.266
      B             1.47
      C             1.42
      D             0.920

     Hz     ppm     Int.

    921.75   2.307     96
    914.67   2.289    103
    911.38   2.281     94
    908.20   2.273    152
    905.64   2.267    166
    903.08   2.260    105
    900.88   2.255    106
    891.85   2.232    124
    603.64   1.511     76
    601.44   1.505     72
    595.95   1.492    129
    594.12   1.487    129
    587.04   1.469    150
    580.44   1.453    171
    577.03   1.444    149
    574.34   1.438    207
    567.38   1.420    219
    560.42   1.403    181
    553.10   1.384     94
    546.51   1.368     31
    374.39   0.937    524
    367.43   0.920   1000
    360.11   0.902    395

in DMSO-d6