2362-10-9

1,3-二(氯甲基)-1,1,3,3-四甲基二硅氧烷(2362-10-9)核磁图(¹³CNMR)

产品名称:1,3-二(氯甲基)-1,1,3,3-四甲基二硅氧烷

CAS:2362-10-9

分子式:C6H16Cl2OSi2

分子量: 231.27

InChI:InChI=1S/C6H16Cl2OSi2/c1-10(2,5-7)9-11(3,4)6-8/h5-6H2,1-4H3

InChIKey: NBGGEWGFZUDQKZ-UHFFFAOYSA-N

Smiles:[Si](CCl)(C)(C)O[Si](CCl)(C)C

Mass

MS-NW-1229          
1,3-bis(chloromethyl)-1,1,3,3-tetramethyldisiloxane
C6H16Cl2OSi2        (Mass of molecular ion:    230)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      28.0       4.3
      29.0       1.0
      43.0       4.1
      44.0       1.5
      45.0       3.3
      51.0       1.1
      52.0       2.8
      59.0       6.4
      63.0       2.1
      65.0       1.9
      66.0      10.5
      66.5       1.6
      73.0       8.2
      75.0       1.0
      79.0       5.9
      81.0       2.3
      87.0       1.1
      92.0       1.3
      93.0       9.2
      94.0       1.1
      95.0       3.6
     107.0       1.5
     115.0       2.2
     117.0       2.5
     123.0       1.9
     125.0       1.1
     131.0       2.5
     137.0       6.4
     139.0       3.6
     151.0       2.1
     153.0     100.0
     154.0      14.1
     155.0      40.9
     156.0       5.2
     157.0       2.8
     159.0      12.5
     160.0       1.4
     161.0       8.5
     162.0       1.0
     163.0       1.9
     173.0       3.8
     175.0       2.6
     181.0      56.7
     182.0       8.7
     183.0      22.3
     184.0       3.3
     185.0       1.5
     187.0       5.9
     189.0       4.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₆ Cl₂ O Si₂	0.04 ml : 0.5 ml CDCl₃
1,3-bis(chloromethyl)-1,1,3,3-tetramethyldisiloxane

    Assign.     Shift(ppm)

      A             2.740
      B             0.220
     
     J(SI-29,B)=6.8HZ.

     Hz     ppm     Int.

    245.38   2.740    329
     23.13   0.259     35
     19.69   0.220   1000
     16.19   0.181     41

in CDCl3

CCl4 solution

liquid film

更多供应商

Capot Chemical Co., Ltd

Shanghai Enchem Industry Co., Ltd.

1,3-二(氯甲基)-1,1,3,3-四甲基二硅氧烷(2362-10-9)核磁图(13CNMR)

1,3-二(氯甲基)-1,1,3,3-四甲基二硅氧烷(2362-10-9)核磁图(¹³CNMR)