2432-14-6

2,6-二溴-4-甲基苯酚(2432-14-6)核磁图(¹³CNMR)

产品名称:2,6-二溴-4-甲基苯酚

CAS:2432-14-6

分子式:C7H6Br2O

分子量: 265.93

InChI:InChI=1S/C7H6Br2O/c1-4-2-5(8)7(10)6(9)3-4/h2-3,10H,1H3

InChIKey: FIGPGTJKHFAYRK-UHFFFAOYSA-N

Smiles:C1(O)=C(Br)C=C(C)C=C1Br

Mass

MS2014-05027CW      
2,6-dibromo-4-methylphenol
C7H6Br2O            (Mass of molecular ion:    264)

   Source Temperature: 250 °C
   Sample Temperature:  25 °C
   Direct, 70 eV

      15.0       2.1
      17.0       6.7
      18.0       2.0
      25.0       1.4
      26.0       4.6
      27.0       9.4
      28.0       1.6
      29.0       3.4
      37.0       7.4
      38.0      16.0
      38.5       1.8
      39.0      10.8
      43.0       2.3
      49.0       6.0
      50.0      31.4
      51.0      58.1
      52.0      11.6
      52.5       1.7
      53.0      25.0
      54.0       1.4
      55.0       1.5
      60.0       1.2
      61.0       7.1
      62.0      10.4
      63.0       8.1
      65.0       1.1
      66.0       2.4
      73.0       3.6
      74.0      12.8
      75.0      17.1
      76.0      12.8
      77.0      68.7
      78.0      38.0
      79.0       7.7
      80.0       3.4
      81.0       5.8
      82.0       3.1
      83.0       1.0
      85.0       1.7
      86.0       2.2
      87.0       1.8
      92.0       1.1
      92.5       6.0
      93.0       1.7
      93.5       5.7
     104.0       2.5
     105.0      14.4
     106.0       9.6
     107.0       1.9
     117.0       1.3
     119.0       1.2
     129.0       1.3
     130.0       1.1
     131.0       2.1
     132.0       1.1
     133.0       2.5
     141.0       1.1
     143.0       1.1
     155.0       3.0
     156.0       4.8
     157.0       5.0
     158.0       4.7
     159.0       2.3
     183.0       3.6
     184.0       1.7
     185.0      80.7
     186.0       7.6
     187.0      75.1
     188.0       5.8
     263.0       6.6
     264.0      51.5
     265.0      16.9
     266.0     100.0
     267.0      14.1
     268.0      49.3
     269.0       3.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₆ Br₂ O	0.047 g : 0.5 ml CDCl₃
2,6-dibromo-4-methylphenol

    Assign.     Shift(ppm)

      A             7.244
      B             5.68
      C             2.244

     Hz     ppm     Int.

    649.75   7.255    257
    649.06   7.248    447
    648.38   7.240    430
    509.00   5.684    388
    201.69   2.253    590
    201.00   2.245   1000
    200.31   2.237    523

in CDCl3