2,2-双(4-氯苯基)-1-乙醇(2642-82-2)核磁图(¹³CNMR)

Mass

MS-NW-8052          
2,2-bis(p-chlorophenyl)ethanol
C14H12Cl2O          (Mass of molecular ion:    266)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       1.2
      51.0       1.4
      63.0       2.4
      73.0       1.1
      75.0       2.3
      81.0       1.1
      81.5       2.3
      82.0       4.7
      82.5       2.1
      89.0       1.8
      99.0       1.7
      99.5       1.2
     101.0       1.3
     111.0       1.0
     113.0       1.0
     125.0       1.7
     139.0       2.1
     163.0       6.6
     164.0       7.3
     165.0      53.4
     166.0       8.7
     199.0      14.5
     200.0       8.7
     201.0       8.4
     202.0       3.2
     203.0       1.2
     231.0       1.9
     233.0       1.1
     235.0     100.0
     236.0      15.9
     237.0      64.8
     238.0      10.1
     239.0      10.9
     240.0       1.6
     266.0      12.7
     267.0       2.0
     268.0       8.2
     269.0       1.2
     270.0       1.4

Assign. Shift(ppm) A 7.285 B 7.156 C 4.134 D 4.098 E 1.59

     Hz     ppm     Int.

   2919.19   7.305     85
   2916.63   7.298    732
   2914.55   7.293    254
   2910.03   7.282    298
   2907.96   7.277   1000
   2905.40   7.270    139
   2866.33   7.173    108
   2863.65   7.166    850
   2861.69   7.161    244
   2857.18   7.150    207
   2855.22   7.145    641
   2852.66   7.138     73
   1661.62   4.158     36
   1656.37   4.145     54
   1653.32   4.137     91
   1648.07   4.124    169
   1640.14   4.104    274
   1634.40   4.090     87
   1632.32   4.085     85
    635.62   1.591     87