2651-46-9

4-氯丁基苯基醚(2651-46-9)红外图谱(IR1)

产品名称:4-氯丁基苯基醚

CAS:2651-46-9

分子式:C10H13ClO

分子量: 184.66

Mass

MS-NW-8628          
4-chlorobutyl phenyl ether
C10H13ClO           (Mass of molecular ion:    184)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      27.0       7.9
      28.0       1.5
      29.0       9.8
      38.0       1.5
      39.0      12.8
      40.0       2.4
      41.0       3.4
      49.0       1.3
      50.0       2.2
      51.0       8.2
      53.0       2.5
      55.0      29.7
      56.0       1.3
      63.0       4.1
      64.0       1.1
      65.0      10.2
      66.0      10.7
      77.0      12.4
      78.0       1.2
      79.0       1.6
      91.0      33.2
      92.0       1.7
      93.0      11.1
      94.0     100.0
      95.0       7.0
     107.0       2.4
     184.0       9.1
     185.0       1.0
     186.0       3.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₃ Cl O	0.05 ml : 0.5 ml CDCl₃
4-chlorobutyl phenyl ether

    Assign.     Shift(ppm)

      A             7.248
      B             6.91
      C             6.87
      D             3.949
      E             3.575
      F          2.06 to 1.80
     
     B AND C WERE CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

    661.44   7.386     42
    659.19   7.361    162
    658.25   7.350    162
    657.31   7.340     96
    656.31   7.329    111
    652.06   7.281    254
    650.69   7.266    442
    648.25   7.239    124
    647.63   7.232    117
    645.19   7.204    220
    643.31   7.184    479
    640.38   7.151     99
    638.31   7.128     37
    627.63   7.008    131
    626.19   6.992    220
    625.13   6.981    236
    621.44   6.939    236
    619.44   6.917   1000
    618.25   6.904    499
    617.50   6.895    498
    615.50   6.873    116
    612.88   6.844    284
    611.75   6.831    279
    610.88   6.821    443
    606.88   6.777     57
    359.69   4.017    224
    358.25   4.001    164
    356.81   3.985    206
    353.81   3.951    632
    352.19   3.933    236
    351.25   3.922    233
    348.06   3.887    234
    346.13   3.865     61
    345.00   3.853     47
    326.63   3.648    194
    324.69   3.626    142
    323.25   3.610    219
    322.38   3.600    234
    320.31   3.577    683
    318.56   3.557    193
    317.31   3.543    199
    315.75   3.526    175
    314.13   3.508    255
    308.63   3.447     31
    187.56   2.095     39
    185.88   2.076     35
    182.81   2.042     85
    179.06   2.000    238
    178.25   1.991    263
    175.13   1.956    599
    172.31   1.924    778
    168.94   1.887    530
    166.06   1.855    290
    162.06   1.810     85
    158.63   1.772     47
    157.56   1.760     46

in CDCl3