2657-87-6

3,4'-二氨基二苯醚(2657-87-6)红外图谱(IR2)

产品名称:3,4'-二氨基二苯醚

CAS:2657-87-6

分子式:C12H12N2O

分子量: 200.24

InChI:InChI=1S/C12H12N2O/c13-9-4-6-11(7-5-9)15-12-3-1-2-10(14)8-12/h1-8H,13-14H2

InChIKey: ZBMISJGHVWNWTE-UHFFFAOYSA-N

Smiles:C1(N)=CC=CC(OC2=CC=C(N)C=C2)=C1

Mass

MS-NW-9477          
3,4'-oxydianiline
C12H12N2O           (Mass of molecular ion:    200)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       1.0
      18.0       5.0
      28.0       1.5
      39.0       4.5
      41.0       1.2
      52.0       2.2
      53.0       3.0
      54.0       1.2
      63.0       1.9
      64.0       1.9
      65.0      11.8
      66.0       2.6
      80.0       9.8
      81.0       1.1
      86.0       2.6
      91.0       1.3
      92.0       3.6
      93.0       9.9
      99.5       1.0
     100.0       6.2
     106.0       1.3
     108.0      27.6
     109.0       5.8
     117.0       1.3
     127.0       1.3
     130.0       2.1
     131.0       1.6
     143.0       1.0
     144.0       2.8
     145.0       1.7
     154.0       3.1
     155.0       2.3
     156.0       4.7
     157.0       1.0
     171.0      16.3
     172.0      17.2
     173.0       2.1
     182.0       2.2
     183.0       2.9
     198.0       1.0
     199.0       6.7
     200.0     100.0
     201.0      14.1
     202.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₂ N₂ O	0.034 g : 0.5 ml CDCl₃
3,4'-oxydianiline

    Assign.     Shift(ppm)

      A             7.027
      B             6.857
      C             6.642
      D             6.32
      E             6.226
      F             3.60

     Hz     ppm     Int.

   2816.77   7.049    275
   2808.72   7.028    563
   2800.66   7.008    311
   2749.15   6.879     80
   2745.73   6.871    759
   2743.41   6.865    279
   2739.14   6.854    305
   2736.82   6.849   1000
   2733.52   6.840    121
   2662.35   6.662    113
   2658.94   6.654    940
   2656.62   6.648    320
   2654.30   6.642     54
   2652.34   6.637    285
   2650.02   6.631    823
   2646.73   6.623     91
   2530.88   6.333    150
   2530.03   6.331    345
   2529.05   6.329    389
   2527.83   6.326    437
   2526.73   6.323    374
   2525.88   6.321    188
   2522.83   6.313    169
   2521.97   6.311    302
   2520.87   6.308    377
   2519.90   6.306    424
   2518.68   6.303    336
   2517.82   6.301    193
   2490.60   6.232    350
   2488.40   6.227    567
   2486.21   6.221    282
   1436.77   3.596    286

in CDCl3