27361-16-6

2-正丁氧基吡啶(27361-16-6)红外图谱(IR1)

产品名称:2-正丁氧基吡啶

CAS:27361-16-6

分子式:C9H13NO

分子量: 151.21

InChI:InChI=1S/C9H13NO/c1-2-3-8-11-9-6-4-5-7-10-9/h4-7H,2-3,8H2,1H3

InChIKey: OFLSKXBALZCMCX-UHFFFAOYSA-N

Smiles:C1(OCCCC)=NC=CC=C1

Mass

MS-KW-0084          
2-butoxypyridine
C9H13NO             (Mass of molecular ion:    151)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       6.7
      28.0       4.8
      29.0      10.7
      38.0       1.8
      39.0      11.5
      40.0       2.6
      41.0      14.9
      42.0       1.0
      50.0       1.4
      51.0       8.4
      52.0       4.6
      53.0       1.8
      55.0       2.7
      56.0       5.0
      57.0       2.0
      66.0       2.5
      67.0      31.4
      68.0       2.2
      78.0      30.8
      79.0      18.8
      80.0       5.1
      93.0       1.8
      94.0       1.1
      95.0     100.0
      96.0      24.3
      97.0       1.6
     106.0       1.9
     107.0       1.0
     108.0      20.2
     109.0       2.7
     121.0      13.7
     122.0      16.1
     123.0       1.3
     150.0       1.3
     151.0       6.2
     152.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₃ N O	0.05 ml : 0.5 ml CDCl₃
2-butoxypyridine

    Assign.     Shift(ppm)

      A             8.141
      B             7.524
      C             6.815
      D             6.712
      E             4.286
      F             1.756
      G             1.480
      J             0.969

     Hz     ppm     Int.

   3257.69   8.152    136
   3256.96   8.150    144
   3255.74   8.147    148
   3254.88   8.145    142
   3252.69   8.139    138
   3251.83   8.137    147
   3250.61   8.134    146
   3249.88   8.132    137
   3015.99   7.547    144
   3014.04   7.542    143
   3008.91   7.529    160
   3007.69   7.526    173
   3006.96   7.524    172
   3005.62   7.521    159
   3000.61   7.509    158
   2998.54   7.503    155
   2730.22   6.832    159
   2729.37   6.830    168
   2725.22   6.820    161
   2724.24   6.817    176
   2723.14   6.814    166
   2722.29   6.812    161
   2718.14   6.802    148
   2717.16   6.799    154
   2687.74   6.726    184
   2686.89   6.724    299
   2685.91   6.721    181
   2679.32   6.705    178
   2678.47   6.703    297
   2677.61   6.700    175
   1719.85   4.304    382
   1713.13   4.287    687
   1706.42   4.270    385
    716.19   1.793     83
    709.72   1.776    188
    709.11   1.775    194
    706.67   1.769     80
    703.25   1.760    192
    702.27   1.758    238
    701.17   1.755    149
    699.95   1.752    145
    696.53   1.743     86
    694.34   1.738    212
    687.74   1.721     99
    609.62   1.526     55
    604.00   1.512     47
    602.29   1.508    166
    596.56   1.493    102
    594.60   1.488    232
    589.11   1.475    102
    587.04   1.469    239
    581.79   1.456     45
    579.71   1.451    158
    572.39   1.433     49
    394.41   0.987    571
    387.08   0.969   1000
    379.64   0.950    493

in CDCl3