1-吡啶-4-哌啶(2767-90-0)核磁图(¹³CNMR)

Mass

MS-NW-9941          
4-piperidinopyridine
C10H14N2            (Mass of molecular ion:    162)

   Source Temperature: 130 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      27.0       1.7
      28.0       1.8
      29.0       1.3
      39.0       2.7
      41.0       2.8
      42.0       1.6
      50.0       1.1
      51.0       7.5
      52.0       2.2
      53.0       1.2
      55.0       3.0
      65.0       1.2
      66.0       1.2
      67.0       1.1
      78.0      11.3
      79.0       2.8
      80.0       1.0
      84.0       1.3
      92.0       1.8
      93.0       1.2
     105.0      11.6
     106.0      22.2
     107.0       7.0
     119.0       2.8
     120.0       1.2
     121.0      15.6
     122.0       1.3
     131.0       1.5
     132.0       1.7
     133.0       8.5
     134.0       1.3
     145.0       1.0
     147.0       3.2
     159.0       1.6
     160.0       1.6
     161.0     100.0
     162.0      79.4
     163.0      11.5

Assign. Shift(ppm) A 8.225 B 6.633 C 3.32 D 1.65 to 1.62

     Hz     ppm     Int.

   3290.53   8.234    263
   3284.06   8.218    265
   2654.30   6.642    415
   2652.71   6.638    292
   2649.17   6.629    301
   2647.58   6.625    399
   1331.18   3.331    321
   1326.05   3.319    519
    667.60   1.671     30
    655.52   1.641   1000
    649.17   1.625    198