28291-10-3

DL-TRANS-4-CHLOROSTILBENEOXIDE(28291-10-3)核磁图(¹HNMR)

产品名称:DL-TRANS-4-CHLOROSTILBENEOXIDE

CAS:28291-10-3

分子式:C14H11ClO

分子量: 230.69

Mass

MS-IW-0842          
(+-)-trans-2-(p-chlorophenyl)-3-phenyloxirane
C14H11ClO           (Mass of molecular ion:    230)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       2.6
      50.0       2.0
      51.0       4.7
      62.0       1.6
      63.0       6.1
      64.0       1.6
      65.0       1.8
      74.0       1.1
      75.0       4.1
      76.0       2.2
      77.0      13.7
      78.0       1.3
      81.5       1.1
      82.0       4.3
      82.5       3.4
      83.0       3.1
      88.0       1.0
      89.0      36.3
      90.0      23.2
      91.0       4.9
     105.0      45.7
     106.0       4.4
     111.0       8.7
     113.0       3.1
     115.0       1.5
     118.0       2.6
     122.0       1.4
     124.0       8.2
     125.0       3.1
     126.0       3.1
     127.0       1.1
     139.0      40.4
     140.0       3.5
     141.0      13.1
     142.0       1.2
     152.0       5.0
     153.0       1.0
     163.0       2.2
     164.0       3.1
     165.0      38.0
     166.0      42.7
     167.0      31.5
     168.0       4.1
     177.0       3.9
     178.0       5.7
     179.0       3.1
     181.0       3.0
     193.0       1.4
     194.0       7.3
     195.0      47.7
     196.0       7.4
     199.0       1.4
     200.0       1.4
     201.0     100.0
     202.0      17.1
     203.0      33.4
     204.0       5.4
     212.0       5.0
     213.0       1.9
     214.0       4.3
     215.0       2.1
     216.0       9.7
     217.0       1.8
     218.0       3.1
     229.0      10.0
     230.0      35.3
     231.0       8.6
     232.0      11.8
     233.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₁ Cl O	0.037 g : 0.5 ml CDCl₃
(+-)-trans-2-(p-chlorophenyl)-3-phenyloxirane

    Assign.     Shift(ppm)

      A          7.37 to 7.33
      B             7.27
      C     *1      3.837
      D     *1      3.813

     Hz     ppm     Int.

   2959.35   7.405     81
   2957.28   7.400    109
   2955.69   7.396     78
   2952.27   7.388    197
   2950.20   7.382    228
   2948.49   7.378    210
   2946.29   7.373    175
   2943.73   7.366    456
   2942.87   7.364    442
   2941.65   7.361    262
   2939.33   7.355    640
   2937.74   7.351    444
   2933.47   7.341    862
   2932.25   7.338    524
   2930.91   7.334   1000
   2928.59   7.328    256
   2927.37   7.325    275
   2925.78   7.321    276
   2921.88   7.312     78
   2916.87   7.299     61
   2914.31   7.293     71
   2910.89   7.284    160
   2908.57   7.278    738
   2906.62   7.273    234
   2902.10   7.262    183
   2900.15   7.257    435
   2897.83   7.251     98
   2895.02   7.244     76
   2893.31   7.240    218
   2891.85   7.236     64
   2890.75   7.234     47
   2888.79   7.229     54
   1534.55   3.840    303
   1532.71   3.836    425
   1524.78   3.816    435
   1522.95   3.811    325

in CDCl3

KBr disc

nujol mull

更多供应商

DL-TRANS-4-CHLOROSTILBENEOXIDE(28291-10-3)核磁图(1HNMR)

DL-TRANS-4-CHLOROSTILBENEOXIDE(28291-10-3)核磁图(¹HNMR)