3069-29-2

N-氨乙基-3-氨丙基甲基二甲氧基硅烷(3069-29-2)核磁图(¹³CNMR)

产品名称:N-氨乙基-3-氨丙基甲基二甲氧基硅烷

CAS:3069-29-2

分子式:C8H22N2O2Si

分子量: 206.36

InChI:InChI=1S/C8H22N2O2Si/c1-11-8(12-2)13-7-3-5-10-6-4-9/h8,10H,3-7,9,13H2,1-2H3

InChIKey: XFFPIAQRIDTSIZ-UHFFFAOYSA-N

Smiles:C(NCCC[SiH2]C(OC)OC)CN

Mass

MS-NW-1356          
(3-(2-aminoethylamino)propyl)dimethoxy(methyl)silane
C8H22N2O2Si         (Mass of molecular ion:    206)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       3.3
      18.0       2.0
      27.0       1.0
      28.0       5.9
      29.0       5.6
      30.0       8.4
      31.0      11.7
      32.0       8.4
      41.0       2.1
      42.0       2.9
      43.0       4.3
      44.0      19.6
      45.0       5.2
      56.0       2.1
      58.0       2.1
      59.0       7.6
      60.0       1.3
      61.0       2.7
      63.0       1.0
      70.0       1.1
      73.0      10.1
      74.0       2.0
      75.0      20.7
      76.0       2.1
      77.0       1.3
      85.0       1.8
      87.0       1.0
      88.0       1.5
      90.0       2.4
      91.0       3.3
      98.0       1.1
      99.0       1.8
     100.0       1.1
     101.0       1.1
     102.0       3.5
     104.0       1.3
     105.0      27.2
     106.0       2.6
     107.0       1.1
     112.0       1.8
     113.0       1.1
     114.0      35.1
     115.0       4.5
     116.0       2.3
     121.0       2.8
     130.0       2.4
     131.0       1.0
     132.0       5.8
     133.0       1.2
     137.0       1.0
     141.0       1.3
     142.0       2.1
     143.0       1.4
     144.0     100.0
     145.0      12.7
     146.0       4.7
     147.0       1.1
     159.0       2.7
     160.0       2.4
     176.0      30.0
     177.0       4.2
     178.0       1.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₂₂ N₂ O₂ Si	0.04 ml : 0.5 ml CDCl₃
(3-(2-aminoethylamino)propyl)dimethoxy(methyl)silane

    Assign.     Shift(ppm)

      A             3.512
      B          2.90 to 2.52
      C             1.56
      D             1.24
      E             0.64
      F             0.117

     Hz     ppm     Int.

    314.56   3.513   1000
    250.88   2.802     38
    250.13   2.793     31
    246.94   2.758     48
    246.19   2.749     56
    242.94   2.713     59
    242.13   2.704     70
    238.94   2.668     32
    238.19   2.660     41
    234.75   2.622     44
    233.50   2.608     32
    227.50   2.541     34
    111.31   1.243    139
     65.13   0.728     28
     10.50   0.118    259

in CDCl3