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321-38-0

1-氟萘(321-38-0)Raman光谱

产品名称:1-氟萘

CAS:321-38-0

分子式:C10H7F

分子量: 146.16

InChI:InChI=1S/C10H7F/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7H

InChIKey: CWLKTJOTWITYSI-UHFFFAOYSA-N

Smiles:C1(F)=C2C(C=CC=C2)=CC=C1

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    Mass

    MS-NW-5447          
    1-fluoronaphthalene
    C10H7F              (Mass of molecular ion:    146)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          50.0       2.3
          51.0       1.7
          60.0       2.5
          62.0       1.3
          63.0       2.2
          72.0       1.3
          73.0       5.7
          74.0       2.8
          75.0       3.5
          94.0       1.7
          96.0       1.8
          98.0       1.1
          99.0       2.4
         120.0       6.1
         125.0       5.6
         126.0       3.8
         127.0       1.0
         144.0       3.2
         145.0       7.2
         146.0     100.0
         147.0      11.1
    

90 MHz in CDCl3

400 MHz in CDCl3

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    1H NMR 89.56 MHz
    C10 H7 F 0.04 ml : 0.5 ml CDCl3
    1-fluoronaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.08 B 7.80 C 7.55 D *1 7.50 E *1 7.48 G 7.31 J 7.11

         Hz     ppm     Int.
    

        729.50   8.146    130
        726.75   8.115    126
        726.13   8.108    151
        724.56   8.091    101
        723.88   8.083    100
        723.19   8.075     69
        722.44   8.067     94
        721.50   8.057     73
        719.88   8.038    187
        706.13   7.885     67
        705.75   7.881     70
        705.38   7.877     70
        705.00   7.872     66
        704.00   7.861     76
        703.19   7.852     98
        701.63   7.835    107
        699.50   7.811    167
        697.50   7.789    136
        696.19   7.774    133
        695.81   7.770    127
        694.38   7.754    137
        692.44   7.732     57
        684.31   7.641    115
        683.88   7.637    130
        683.44   7.632    155
        682.44   7.620    128
        678.88   7.581    101
        678.00   7.571     99
        676.19   7.551    276
        674.88   7.536   1000
        672.06   7.505    302
        671.25   7.495    395
        668.88   7.469    319
        668.06   7.460    410
        666.56   7.443     48
        665.31   7.429    612
        662.56   7.398    229
        660.44   7.375    353
        655.06   7.315    305
        652.38   7.285    197
        646.94   7.224    192
        645.50   7.208    251
        643.94   7.191    242
        638.06   7.125    120
        636.44   7.107    104
        634.88   7.089    235
        633.56   7.075    235
        627.38   7.006    129
        626.06   6.991    122
    

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    1H NMR 399.65 MHz
    C10 H7 F 0.05 ml : 0.5 ml CDCl3
    1-fluoronaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.09 B 7.80 C 7.564 D *1 7.49 E *1 7.47 G 7.331 J 7.103 J(F-19,G) = 5.4 HZ. J(F-19,J) = 10.7 HZ. J(G,J)= 7.7 HZ. J(C,J)= 1.0 HZ. J(C,G) = 8.3 HZ.

         Hz     ppm     Int.
    

       3242.68   8.114     31
       3240.36   8.108     71
       3237.30   8.101    347
       3235.11   8.095    240
       3233.03   8.090    305
       3227.66   8.077    403
       3124.39   7.818     66
       3121.95   7.812    230
       3120.24   7.808    344
       3118.65   7.804    209
       3116.70   7.799    255
       3115.11   7.795    293
       3112.92   7.790    355
       3110.72   7.784    275
       3107.18   7.775     72
       3027.59   7.576    567
       3019.29   7.555    678
       3010.38   7.533     30
       3006.59   7.524     41
       3004.52   7.518     40
       3000.98   7.510     98
       2998.90   7.504    192
       2994.14   7.492    626
       2992.55   7.488    870
       2988.53   7.478   1000
       2984.50   7.468    715
       2983.03   7.465    677
       2978.27   7.453    188
       2976.20   7.448    100
       2973.39   7.440     33
       2973.02   7.440     33
       2972.17   7.437     34
       2940.31   7.358    325
       2934.94   7.344    339
       2932.50   7.338    463
       2927.12   7.325    461
       2924.44   7.318    342
       2918.95   7.304    318
       2848.02   7.127    369
       2847.05   7.124    403
       2840.33   7.108    335
       2839.36   7.105    363
       2837.28   7.100    396
       2836.30   7.097    414
       2829.59   7.081    317
       2828.74   7.079    344
    

in CDCl3

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liquid film

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