2,6-二溴-4-氟苯胺(344-18-3)核磁图(¹³CNMR)

Mass

MS-KW-0416          
2,6-dibromo-4-fluoroaniline 
C6H4Br2FN           (Mass of molecular ion:    267)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       1.6
      31.0       4.3
      37.0       1.9
      38.0       1.6
      44.5       1.1
      50.0       1.0
      51.0       1.1
      52.0       5.6
      53.5       1.5
      54.0       1.4
      54.5      14.0
      55.0       1.8
      56.0       3.3
      57.0       3.2
      61.0       3.6
      62.0       3.8
      63.0       2.5
      64.0       1.0
      65.0       1.5
      80.0       2.8
      81.0      13.3
      82.0       8.9
      83.0       1.3
      89.0       2.6
      93.5       3.3
      94.0       3.6
      94.5       3.6
      95.0       3.4
     107.0       2.6
     108.0      48.0
     109.0      25.7
     110.0       1.7
     133.5       4.5
     134.5       8.5
     135.0       1.4
     135.5       4.2
     160.0       1.1
     161.0       3.3
     162.0       1.2
     163.0       2.8
     187.0       4.0
     188.0      10.8
     189.0       4.7
     190.0       9.9
     241.0       1.0
     267.0      51.4
     268.0       4.5
     269.0     100.0
     270.0       7.5
     271.0      48.9
     272.0       3.5

Assign. Shift(ppm) A 7.187 B 4.37

     Hz     ppm     Int.

   2876.84   7.196   1000
   2869.02   7.177    982
   2865.73   7.169     23
   1747.32   4.371    122