3490-06-0

N-甲基-2-(3,4-二甲氧基苯基)乙胺(3490-06-0)红外图谱(IR1)

产品名称:N-甲基-2-(3,4-二甲氧基苯基)乙胺

CAS:3490-06-0

分子式:C11H17NO2

分子量: 195.26

InChI:InChI=1S/C11H17NO2/c1-12-7-6-9-4-5-10(13-2)11(8-9)14-3/h4-5,8,12H,6-7H2,1-3H3

InChIKey: HNJWKRMESUMDQE-UHFFFAOYSA-N

Smiles:C1(CCNC)=CC=C(OC)C(OC)=C1

¹HNMR

IR1

Mass

MS-IW-3474          
3,4-dimethoxy-n-methylphenethylamine
C11H17NO2           (Mass of molecular ion:    195)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      28.0       1.8
      39.0       2.8
      42.0       4.3
      43.0       1.6
      44.0     100.0
      45.0       4.3
      51.0       3.1
      52.0       1.3
      53.0       1.0
      58.0      14.1
      63.0       1.4
      65.0       4.0
      77.0       4.0
      78.0       3.6
      79.0       2.2
      89.0       1.4
      90.0       1.6
      91.0       3.7
     105.0       2.2
     106.0       3.3
     107.0       4.6
     108.0       1.7
     109.0       1.9
     118.0       1.0
     121.0       2.0
     135.0       1.3
     137.0       6.5
     151.0      10.8
     152.0      62.5
     153.0       6.3
     164.0       1.2
     165.0       1.1
     195.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₇ N O₂	0.05 ml : 0.5 ml CDCl₃
3,4-dimethoxy-N-methylphenethylamine

    Assign.     Shift(ppm)

      A             6.788
      B             6.75
      C             6.74
      D     *1      3.855
      E     *1      3.830
      F             2.815
      G             2.747
      J             2.424
      K             1.99

     Hz     ppm     Int.

   2718.99   6.804    115
   2714.23   6.792     34
   2710.33   6.782    245
   2698.12   6.752     93
   2696.17   6.747    200
   2694.34   6.742    231
   2692.50   6.738    187
   2689.58   6.730    107
   2687.62   6.725     52
   1540.65   3.855    974
   1530.88   3.831   1000
   1133.79   2.837     40
   1132.20   2.833     44
   1125.49   2.817    127
   1119.26   2.801    117
   1103.64   2.762    154
   1097.53   2.747    179
   1091.06   2.731     57
   1089.11   2.726     53
    968.99   2.425    667
    794.92   1.990     55

liquid film