35182-51-5

4-(3-戊基)吡啶(35182-51-5)质谱(MS)

产品名称:4-(3-戊基)吡啶

CAS:35182-51-5

分子式:C10H15N

分子量: 149.23

InChI:InChI=1S/C10H15N/c1-3-9(4-2)10-5-7-11-8-6-10/h5-9H,3-4H2,1-2H3

InChIKey: YHXYCIZBTSECRP-UHFFFAOYSA-N

Smiles:C1=NC=CC(C(CC)CC)=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-6641          
4-(1-ethylpropyl)pyridine
C10H15N             (Mass of molecular ion:    149)

   Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.2
      26.0       1.0
      27.0       5.3
      28.0       1.9
      29.0       3.5
      39.0       8.0
      40.0       1.0
      41.0       7.7
      50.0       2.2
      51.0       8.3
      52.0       4.0
      53.0       2.6
      54.0       1.6
      63.0       2.4
      64.0       1.0
      65.0       9.9
      66.0       1.4
      77.0       5.4
      78.0       4.5
      79.0       2.8
      80.0       2.8
      91.0       4.6
      92.0      70.6
      93.0       9.9
      94.0       1.0
     104.0       2.8
     105.0       2.4
     106.0       7.7
     107.0       1.4
     117.0       3.1
     118.0       9.0
     119.0       7.6
     120.0     100.0
     121.0      13.5
     134.0       7.6
     135.0       1.0
     148.0       2.5
     149.0      49.7
     150.0       5.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₅ N	0.05 ml : 0.5 ml CDCl₃
4-(1-ethylpropyl)pyridine

    Assign.     Shift(ppm)

      A             8.487
      B             7.064
      C             2.305
      D             1.61
      E             0.768

     Hz     ppm     Int.

    763.31   8.523    288
    761.69   8.505    185
    758.88   8.474    196
    757.25   8.456    310
    635.50   7.096    305
    633.94   7.079    187
    631.06   7.047    179
    629.44   7.029    269
    214.00   2.390     36
    208.50   2.329     72
    205.13   2.291     35
    203.00   2.267     46
    199.88   2.232     55
    194.38   2.171     33
    162.56   1.816     55
    160.56   1.793     30
    157.50   1.759     65
    154.69   1.728    129
    150.25   1.678    167
    149.06   1.665    139
    147.06   1.643    155
    143.06   1.598    194
    141.50   1.580    181
    139.88   1.562    105
    136.50   1.525    112
    134.44   1.502    149
    130.81   1.461     34
    129.50   1.446     45
    127.88   1.428     71
     75.31   0.841    532
     68.31   0.763   1000
     60.81   0.679    333

in CDCl3