35386-24-4

1-(2-甲氧苯基)哌嗪(35386-24-4)核磁图(¹³CNMR)

产品名称:1-(2-甲氧苯基)哌嗪

CAS:35386-24-4

分子式:C11H16N2O

分子量: 192.26

InChI:InChI=1S/C11H16N2O/c1-14-11-5-3-2-4-10(11)13-8-6-12-7-9-13/h2-5,12H,6-9H2,1H3

InChIKey: VNZLQLYBRIOLFZ-UHFFFAOYSA-N

Smiles:N1(C2=CC=CC=C2OC)CCNCC1

Mass

MS-NW-6701          
1-(o-methoxyphenyl)piperazine
C11H16N2O           (Mass of molecular ion:    192)

   Source Temperature: 100 °C
   Sample Temperature:  90 °C
   Reservoir, 75 eV

      15.0       1.6
      18.0       1.1
      27.0       2.4
      28.0       7.8
      29.0       5.5
      30.0       4.3
      39.0       2.9
      41.0       1.5
      42.0       3.4
      51.0       2.8
      52.0       1.4
      56.0      10.8
      57.0       5.4
      63.0       1.4
      64.0       1.3
      65.0       5.3
      77.0       4.1
      78.0       2.0
      79.0       1.8
      91.0       2.9
      92.0       2.4
      93.0       1.9
     104.0       1.2
     106.0       2.2
     107.0       1.5
     120.0       9.6
     121.0       4.9
     122.0       1.2
     134.0       8.0
     135.0      11.9
     136.0       4.9
     137.0       2.0
     150.0     100.0
     151.0      10.0
     191.0       1.2
     192.0      50.9
     193.0       7.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₁₆ N₂ O	0.038 g : 0.5 ml CDCl₃
1-(o-methoxyphenyl)piperazine

    Assign.     Shift(ppm)

      A          6.99 to 6.85
      B             3.853
      C             3.04
      D             1.81

     Hz     ppm     Int.

    625.75   6.987     34
    622.50   6.951    103
    621.25   6.937    275
    620.69   6.931    300
    618.69   6.909    116
    617.56   6.896    137
    615.63   6.874     46
    615.19   6.870     48
    613.81   6.854     27
    612.63   6.841     24
    345.13   3.854    759
    277.94   3.104     24
    276.81   3.091     29
    276.13   3.084     32
    272.00   3.038   1000
    162.56   1.816    134

in CDCl3