9,10-dibenzylanthracene (3613-42-1)核磁图(¹³CNMR)

Mass

MS-IW-1081          
9,10-dibenzylanthracene
C28H22              (Mass of molecular ion:    358)

   Source Temperature: 190 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      91.0       1.5
     103.0       1.4
     126.0       1.4
     131.5       1.0
     132.5       3.9
     133.0       1.0
     138.0       1.0
     139.0       3.5
     139.5       1.1
     140.0       4.3
     140.5       1.0
     163.0       1.6
     165.0       1.5
     169.5       1.0
     178.0       1.9
     179.0       1.7
     189.0       1.6
     202.0       4.0
     203.0       4.7
     204.0       1.1
     239.0       1.5
     252.0      12.4
     253.0       3.6
     263.0       2.6
     264.0       1.3
     265.0      22.7
     266.0      11.1
     267.0      42.0
     268.0      10.5
     269.0       1.5
     276.0       2.0
     277.0       2.0
     278.0       2.5
     279.0       5.3
     280.0       3.1
     281.0       9.6
     282.0       2.2
     356.0       1.0
     357.0       1.4
     358.0     100.0
     359.0      30.9
     360.0       4.7

Assign. Shift(ppm) A 8.262 B 7.427 C 7.206 D 7.15 to 7.12 E 5.037

     Hz     ppm     Int.

   3310.91   8.285     63
   3309.81   8.282     83
   3307.25   8.276    569
   3303.96   8.268    441
   3300.29   8.258    439
   3297.00   8.250    612
   3294.43   8.244     89
   3293.33   8.241     71
   2977.05   7.450     76
   2975.95   7.447     99
   2973.39   7.440    649
   2970.09   7.432    482
   2966.43   7.423    489
   2963.13   7.415    620
   2960.57   7.408     87
   2959.47   7.406     69
   2890.87   7.234     37
   2889.40   7.230    113
   2888.18   7.227    189
   2886.35   7.223    123
   2884.16   7.217    301
   2881.96   7.212    251
   2880.74   7.209    411
   2879.76   7.206    340
   2873.78   7.191    608
   2860.23   7.157    483
   2858.64   7.153    643
   2855.83   7.146    264
   2853.39   7.140    344
   2850.83   7.134    352
   2846.68   7.123    116
   2013.31   5.038   1000