38762-41-3

4-溴-2-氯苯胺(38762-41-3)核磁图(¹³CNMR)

产品名称:4-溴-2-氯苯胺

CAS:38762-41-3

分子式:C6H5BrClN

分子量: 206.47

Mass

MS-KW-0279          
4-bromo-2-chloroaniline
C6H5BrClN           (Mass of molecular ion:    205)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       2.5
      36.0       1.0
      37.0       3.4
      38.0       4.4
      39.0       3.9
      40.0       1.2
      41.0       3.6
      44.5       6.5
      45.0       2.7
      45.5       5.1
      49.0       1.6
      50.0       2.2
      51.0       1.3
      52.0       7.0
      61.0       4.5
      62.0       7.7
      62.5       7.3
      63.0      22.8
      63.5       2.5
      64.0       6.8
      65.0       3.5
      72.0       1.0
      73.0       4.2
      74.0       2.4
      75.0       2.5
      84.5       1.2
      85.5       1.2
      88.0       1.2
      89.0       2.1
      90.0      42.2
      91.0       9.3
      97.0       1.3
      98.0       1.1
      99.0      12.2
     100.0       1.3
     101.0       4.0
     102.5       5.8
     103.5       7.5
     104.5       1.8
     125.0       2.5
     126.0      25.5
     127.0       2.9
     128.0       8.2
     143.0       1.4
     145.0       1.2
     169.0       1.3
     170.0       1.0
     171.0       1.3
     177.0       1.9
     179.0       2.5
     205.0      77.0
     206.0       6.3
     207.0     100.0
     208.0       7.3
     209.0      24.1
     210.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₅ Br Cl N	0.035 g : 0.5 ml CDCl₃
4-bromo-2-chloroaniline

    Assign.     Shift(ppm)

      A             7.370
      B             7.149
      C             6.628
      D             4.05

     Hz     ppm     Int.

   2946.78   7.374    840
   2944.58   7.368    874
   2862.67   7.163    478
   2860.47   7.158    452
   2854.13   7.142    516
   2851.93   7.137    489
   2652.83   6.638   1000
   2644.29   6.617    929
   1617.19   4.047    190

in CDCl3